Acetic anhydride

occurs in the liquid phase according to the radical mechanism produced by MEC as the intermediate and acetic acid as the final product. Mice and acetic acid (0.2: 1.0 mass ratio) are obtained by non-oxidizing liquid phase oxidation at 1800C and 53 bars with remixing. Continuous oxidation under the flow conditions of components at 1500C, 65 bar and the stay time of 2-7 minutes constitute MEK and acetic acid by 3: 1 mass. This process has a slight economic advantage over the removal of 2-butanol.…

Aims of Experiment 1. To extract benzoic acid from the toluene-benzoic acid mixture, using oxidation-reduction reaction (chemical properties) and difference of solubility (physical properties) –Expt. 1 2. To learn how to recrystallize the solid organic compounds well for getting more purified compounds –Expt. 2 3. To find which differences between raw product and recrystallized product are observed. –Expt. 2 4. To determine melting point range of organic compounds with digital melting point…

RESULTS SOLUBILITY ANALYSIS: Ketoprofen sample was found to be soluble in ethanol, Chloroform, ether, acetone at neutral pH and is found to be almost insoluble in water. Solubility analysis is important because the drug has to dissolve in the solvents and also in the dissolution medium used. MELTING POINT DETERMINATION: The melting point of the Ketoprofen was found to be 96˚C by open capillary tube using microcontroller based melting point apparatus which is within the reported range of 94˚C…

After deprotonation of 6.8 mmol naphthalen-2-ol by 14.0 mmol NaOH, the resulting anion was placed together with 8.8 mmol 1-iodobutane, and the reaction was performed by reflux in 20 mL of ethanol (EtOH) solvent, and the product was allowed to cool on ice and collected by suction filtration. The final crystals had a very pale amber color and were odorless. The following week, after being allowed to completely dry for a week at room temperature, the IR spectrum of the product in liquid suspension…

RESULT AND DISCUSSION 7.1. Preformulation studies 7.1.1. Identification of pure drug by FTIR Figure7.1: Identification of Sample through FTIR Figure 7.2: FTIR Spectrum of Standard Prazosin hydrochloride (with references of B.P.- 2009) Table: 7.1 - Characteristics peaks of Prazosin hydrochloride S.No. Reference peaks (cm-1) Theoretical peak of Prazosin hydrochloride Obtained peaks (cm-1) Functional Group Stretching/ Bending 1 1750-1680 1529.92 1529.92 C=O Stretching 2. 1650-1580…

a) Heckel equation In 1961, Heckel proposed the most widely used equation describing pharmaceutical powder behavior in compaction. It was initially used to study the densification of ceramics and its correlation with pressure. It a first order process where powder pores elimination rate is correlated to the number of pores present. The rate of volume reduction increases as the number of pores decrease. Heckel equation relates the density, pressure and the pore fraction of the powder [16],.…

1. Abstract In this study, reverse micellar extraction of asparaginase model system was carried out using CTAB/Iso-octane/hexanol/butanol system to optimize the forward and back extraction efficiency. By using Taguchi’s orthogonal array (OA), maximum forward extraction efficiency of 55.0%, 61.0% and 54% was achieved with an aqueous phase pH of 11.0, 150mM CTAB/Iso-octane and 0.1 M NaCl, respectively. Similarly, Taguchi’s orthogonal array (OA) was applied to optimize the pH of stripping phase,…

CHAPTER 5 PROPERTIES OF MAHUA METHYL ESTER AND THEIR BLENDS WITH DIESEL 5.1 INTRODUCTION In this work, characteristic fuel properties of mixture of Mahua methyl ester and their blends with diesel in the proportions of 10:90, 25:75, 50:50, 75:25 and 100:0 respectively were studied. The characteristics fuel properties of Mahua methyl ester blends were found to be those of diesel oil. 5.2 MATERIAL AND METHODS The Mahua oil methyl ester was prepared by using three stage transesterification…

Have you ever heard about alkaline water? Do you really know what it is? When it comes to alkaline water, you should know this water is slightly basic. It has basic minerals, including magnesium, calcium and bicarbonate. All these compounds will bind to hydrogen ions in solution, making the water more basic. Moreover, this type of water refers to its pH level, which is a number that measures how alkaline a substance is on a scale of 0-14. For example, if something will have a pH level of 1, it…

For acetic acid-sodium hydroxide titration, 10ml of distilled water was added to 250ml Erlenmeyer flask. 20ml of diluted acetic acid was pipetted into that 250ml Erlenmeyer flask. Titration system that contained 0.100M NaOH in the burette was set up. The pH meter was used to monitor pH of the system when sodium hydroxide…