Acetic anhydride

the plate.5 Thus, compounds are separated according to their differing behavior in the adsorbent-solvent system, with their final heights on the plate and Rf values determined, in general, by their relative degrees of polarity. For best results, acetic acid was a necessary component of the development solvent in this experiment because it was a source of protons, which prevented the…

Table: 9 FT- IR analysis of methanol extract of M. concanensis leaves S. No Peak values Intensity range Intensity Group assignment Functional groups 1 3972.43 0.0086 Unknown 2 3859.33 0.0412 Unknown 3 3805.79 0.0733 Unknown 4 3396.46 0.9280 Medium N-H stretch Amides, alcohols and amines 5 2987.43 0.2450 Medium C-H stretch Alkanes and acids 6 2946.27 0.2810 Medium C-H stretch Alkanes and acids 7 2912.38 0.2040 Medium C-H stretch Alkanes 8 2834.49 0.3170 Weak C-H stretch Aldehydes and…

PRE FORMULATION STUDY: Pre formulation testing was an investigation of physical and chemical properties of a drug substance alone and when combined with excipients. It was the first step in the rational development of dosage forms. Class: -Pre formulation study can divide into two subclasses: API characterization, Compatibility study Active pharmaceutical ingredient (API) characterization:- Organoleptic evaluation:-These are preliminary characteristics of any substance which is useful in…

The heterocyclic compounds naming tetrahydrocarbazoles having the significant biological properties. The newly substituted tetrahydrocarbazole derivatives were prepared from substituted phenylhydrazine and cyclohexanone in glacial acetic acid under reflux. These intermediates on reaction with substituted aromatic acid chlorides in alkaline media finally converted to N-Substituted tetrahydrocarbazoles. Fifteen compounds are synthesized and charaterized by their melting point (MP), IR, NMR, MS…

In this study, we use the modified organo nanoclay as a new sorbent for separation and preconcentration trace amounts of Au(III) in aqueous solutions. Nanoclay was modified with 5-(4'-dimethylamino benzyliden)-rhodanine. Modified nanoclay was used as a solid sorbent for separation and preconcentration trace amounts of Au(III) ions. The sorption of gold ions was quantitative in pH range of 2.0 to 6.0, whereas quantitative desorption occurs instantaneously with 6.0 mL of 1.0 mol L-1 Na2S2O3. The…

The purpose of this lab was to perform reduction of ketones by reducing 4-t-butylcyclohexanone with sodium borohydride (NaBH4) to form 4-t-butylcyclohexanol. At the end of this experiment, the infrared spectroscopy was obtain for the final product, 4-t-butylcyclohexanol. The IR graph showed the presence of the desired product, and it also showed if the reaction went to completion or not. In addition, the mass of the final product was obtained to determine the percent yield. To a 5mL conical…

experiment tested why mixing reactants in different mole ratios affected the amount of the product and the amount of each reactant that is left over. To solve the problem, the lab contained reacting sodium bicarbonate(baking soda) and acetic acid(vinegar) in different ratios and seeing if the product changed. The data suggests that the higher ratio of baking soda to vinegar creates the most product. For the ratio 3:1, the final grams of sodium acetate(product) was 0.09, the product…

The objective of this experiment was to oxidize 9-fluorenol with bleach to form 9-fluorenone. This was done with three different reactions, each under different conditions. The reactions were evaluated using the TLC plate to see how far each reaction progressed. During the experiment reaction test tube 2 had the darkest yellow color out of the three reactions. On the TLC plate the starting material had one dot, with an Rf value of 0.22. Reaction 1 had two dots, with Rf values of 0.29 and…

Sofya Tkachman AP Biology, A2 Dr. Lau 15 September, 2015 Enzyme Catalysis I. Purpose Measure the activity of catalase in potato extract using several different methods. II. Procedure a) Cut 20 small circles from a large filter paper disk using a hole puncher. Clean and dry several medicine cups and pour hydrogen peroxide into one. Put the catalase enzyme, previously prepared by blending a potato, into another medicine cup. Make a 1/8 dilution of the catalase by adding chilled distilled water.…

This lab used techniques in steam distillation to extract crude oil from cloves. The cloves were boiled in a round bottom flask and using a hydrodistillation apparatus, the crude oil was separated from the cloves and sent into a clean flask. This step was used to separate the essential oils from the cloves (Setzer, W., 2008). The distillate was poured into a separatory funnel and extracted three times with dichloromethane to extract the water. After being extracted three times, a fifth of the…