The compound was soluble in water and hydrochloric acid, but was not soluble in sodium hydroxide, toluene, and acetone as indicated by Table 2. For a compound to be soluble it means that the compound must be able to dissolve in a certain liquid. This was proven by using the solubility tests. Since the unknown compound was soluble in water it means that it is a polar or ionic compound, and since it is soluble in hydrochloric acid it means that it is probably an organic base. It was soluble in water because water is a polar molecular and since it’s polar, the molecules interact using hydrogen bonds and dipole-dipole intermolecular forces.…
When solid was formed the product was purified using sublimation. The final product (camphor) was tested for its melting point and an IR spectrum was obtained. To reduce the camphor to isoborneol sodium borohydride was used. Once this…
In the Fischer approach, an acid is used in order to allow the esterification to occur. Gas chromatography separates compounds by their elution time. Data and Results The compound in the gas chromatograph exhibited a retention time of 3.68 minutes.…
Visual comparison of the available solid and aqueous compounds to the unknown was done first so as to eliminate unnecessary testing. A 30.0 g/mL solution of the unknown was made in a beaker by dissolving 1.000 g of the unknown in 30.0 mL of distilled water. Before weighing out 1.000 g of the unknown, the scale was zeroed out with a piece of weighing paper (square cut-out of normal paper) on it. Using a scoopula, 1.000 g was the compound was carefully placed on the weighing paper and measured to exactly 1.000 g. These same measurements and procedures were used when solutions of calcium chloride and nitric acid were created using separate beakers. Portions of each solution were then poured into test tubes (exact measurements were not necessary for this step).…
Once the solubility tests were finished, this provided numerical evidence that aided in determining the identification of the compound. From these three weeks of investigation, the group…
Discussion and Scientific Explanations The main goals of this experiment was to find the unknown compound, to discover the compounds chemical and physical properties and create two synthesis of the compound and compare the two compounds. We found out our compound was ionic because the compound dissolved in water, but not in toluene or acetone by using a solubility test, results on Table 1 of the group lab report. On page 59 of the Cooperative Chemistry Laboratory Manual is a chart on suggested liquids and the inference if the compound is soluble [1]. When then checked the pH of the solution by using pH strip. The solution had a pH>7.…
After each compound was added to the 50mL of water we used a magnetic stirrer and a stir plate to dissolve the compound and then a thermometer to measure both the initial and final temperatures of the compounds. Before we began our experiment it was necessary to look into the MSDS…
Identification of Unknown Compounds 64A and 64B 64A, was a white powdery solid substance. 64B, was a clear colorless liquid that had the smell of alcohol. Solubility analysis is a method of identifying compounds based on how their behavior in other compounds. Solubility is the ability of a solvent to dissolve a solute.…
Table 1 shows this, as well as the disparity of the pH values of the compounds. Chemical Physical Characteristics…
Given an unknown compound in container 3, solubility tests, cation tests, anion tests, and conductivity tests can be used to determine the various properties of the unknown to then make a positive identification of the unknown. These results will not only show chemical and physical properties but also what the unknown compound might react with to form other compounds. After performing the four anion tests, a positive identification was able to be made showing that the unknown compound contained a chloride ion since a white precipitate was formed from the reaction (Table 1). The sulfate, nitrate, and carbonate tests all yielded negative results when no precipitate was formed. The reaction of the chloride anion is as follows: Cl-…
Identifying an Unknown Compound Using Various Chemical Analysis Techniques Joshua Nash and Aquilla Young Abstract The introduction of this lab report exposes the reader to the different scientific concepts that are to be used such as melting point calculations, retention factors, and solubility in various aqueous solutions. The experimental provides the basics of using a melting point apparatus, determining solubility, and performing thin layer chromatography. In the results section the findings of my experimental are tabulated and presented in a well-organized manner so that the reader can understand how each value was calculated.…
In this experiment, solid magnesium was conducted in a chemical reaction with hydrochloric acid solution. The three objectives include: measuring the gas production of a chemical reaction by a pressure change, determining the mass of the hydrogen gas produced in the reaction, and determining the effectiveness of the procedure by calculating the percent yield. In order to complete these objectives, a flask containing the magnesium ribbon was completely submerged into a large beaker filled with water. Next, hydrochloric acid was emptied into the flask using a gas syringe. Then, a Gas Pressure Sensor was used to measure the pressure in the sealed vessel, and a temperature probe was used to measure the temperature of the reaction indirectly by…
An unidentified compound was presented as a challenge to determine what the compound was. Given the unknown compound, the task was to investigate and determine the ions of the compound. To determine the ions, an ion test was performed. Based on physical observations, solubility, and flame observations, the assumption that a halide was present was made, and then this hypothesis was tested. An aqueous solution consisting of 1.000 g of the unknown and 30 mL water was made, and the tests mentioned, as well as conductivity and pH were tested.…
The separated compounds were then classified by determination of their melting points and 1H NMR. Results and Discussion In this…
Discussion For the first part of the experiment, a solubility test was conducted on all compounds. Because they were all ionic, every known compound naturally dissolved in water, and conducted electricity. As the next determining factor in the process to identify the unknown substance, the compounds were tested in acetone. As seen in table 2, only one compound, Ca(NO3)2 was found to be soluble in this solvent.…