Unknown Compound Analysis Essay

Superior Essays
Identifying an Unknown Compound Using Various Chemical Analysis Techniques
Joshua Nash and Aquilla Young
Abstract
The introduction of this lab report exposes the reader to the different scientific concepts that are to be used such as melting point calculations, retention factors, and solubility in various aqueous solutions. The experimental provides the basics of using a melting point apparatus, determining solubility, and performing thin layer chromatography. In the results section the findings of my experimental are tabulated and presented in a well-organized manner so that the reader can understand how each value was calculated. In the discussion an explanation is given that reiterates and further explains how the results were calculated. The lab report is concluded by revealing any experimental errors that may have caused a flaw in the results.
Background
This experiment uses the concept that by calculating the retention factors of an unknown compound by using thin-layer chromatography, recording the melting points, and determining the solubility of that unknown compound, that it is possible to determine what that compound is by comparing it to known compounds that have similar retention factors, melting points, and solubility.
…show more content…
The temperature that the solid compound begins to melt is known as the point of condensation and the point that the solid has completely liquefied is known as the melting point/temperature. Solubility is simply the ability of a solid compound to completely diffuse/dissociate in an aqueous solution. For example, when you add sugar to a glass of water and the sugar diffuses throughout the water, the sugar is said to be soluble in water. On the contrary, when you add oil to water and the oil settles on top of the water, the oil is said to be insoluble, or not soluble in

Related Documents

  • Improved Essays

    Nt1310 Unit 6 Lab

    • 1594 Words
    • 7 Pages

    The compound was soluble in water and hydrochloric acid, but was not soluble in sodium hydroxide, toluene, and acetone as indicated by Table 2. For a compound to be soluble it means that the compound must be able to dissolve in a certain liquid. This was proven by using the solubility tests. Since the unknown compound was soluble in water it means that it is a polar or ionic compound, and since it is soluble in hydrochloric acid it means that it is probably an organic base. It was soluble in water because water is a polar molecular and since it’s polar, the molecules interact using hydrogen bonds and dipole-dipole intermolecular forces.…

    • 1594 Words
    • 7 Pages
    Improved Essays
  • Improved Essays

    Aspirin Powder Lab

    • 352 Words
    • 2 Pages

    Purpose: The purpose of the lab was to identify a powder based on its physical and chemical properties. Materials & Apparatus: -eye protection -well plate -pipette -small toothpick/ paper clip for stirring -6 white powders: icing sugar, cornstarch, Aspirin powder, baking powder, mystery powder -test solutions in dropper bottles: water, universal indicator, vinegar, iodine solution Safety notes: Aspirin Powder- in case of contact with skin, wash with soap and water. Universal indicator- toxic, in case of contact with skin or eyes, rinse for 15 minutes. Iodine- rinse for 15 minutes in case of contact with skin or eyes.…

    • 352 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    In the nine unknown solutions experiment there was nine solutions that were labeled with just numbers from one to nine and all of these one to nine solutions were mixed together randomly to see what kind of reaction it would form. There were mostly no reactions being formed but the reactions that were soluble and insoluble formed different colors of precipitate. The main importance in finding the nine unknown solutions was to prevent any inaccuracies that might form when there is a chemical compound forming. This experiment was done to determine the identity of the nine unknown solutions like color (physical trait), and chemical characteristics.…

    • 791 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Unknown Compounds

    • 695 Words
    • 3 Pages

    Once the solubility tests were finished, this provided numerical evidence that aided in determining the identification of the compound. From these three weeks of investigation, the group…

    • 695 Words
    • 3 Pages
    Improved Essays
  • Great Essays

    Discussion and Scientific Explanations The main goals of this experiment was to find the unknown compound, to discover the compounds chemical and physical properties and create two synthesis of the compound and compare the two compounds. We found out our compound was ionic because the compound dissolved in water, but not in toluene or acetone by using a solubility test, results on Table 1 of the group lab report. On page 59 of the Cooperative Chemistry Laboratory Manual is a chart on suggested liquids and the inference if the compound is soluble [1]. When then checked the pH of the solution by using pH strip. The solution had a pH>7.…

    • 931 Words
    • 4 Pages
    Great Essays
  • Improved Essays

    Unknown Compounds

    • 816 Words
    • 4 Pages

    Given an unknown compound in container 3, solubility tests, cation tests, anion tests, and conductivity tests can be used to determine the various properties of the unknown to then make a positive identification of the unknown. These results will not only show chemical and physical properties but also what the unknown compound might react with to form other compounds. After performing the four anion tests, a positive identification was able to be made showing that the unknown compound contained a chloride ion since a white precipitate was formed from the reaction (Table 1). The sulfate, nitrate, and carbonate tests all yielded negative results when no precipitate was formed. The reaction of the chloride anion is as follows: Cl-…

    • 816 Words
    • 4 Pages
    Improved Essays
  • Superior Essays

    The experiment that I will be conducting focuses on how fast one tablet of Alka seltzer can dissolve in various temperatures of water. The core of this procedure is to determine the impact that temperature has on how fast something dissolves. My hypothesis for this experiment would be that the Alka Seltzer that dissolves the fastest would be the one that was placed in the water with the highest temperature. There will be controlled and manipulated variables explained throughout the experiment. The two main things used in this experiment will be the solute and the solvent, which is Alka Seltzer and water.…

    • 1462 Words
    • 6 Pages
    Superior Essays
  • Great Essays

    Purpose: As derivatives of carboxylic acids, esters are abundant compounds that often contribute to the fragrances in flowers, fruits, and coffee. Esters are synthesized from either organic or inorganic acids through a process called esterification. In this reaction, a carboxylic acid (RCOOH) and an alcohol (R’OH) mix in the presence of a strong acid catalyst to form a neutral, water-insoluble ester (RCOO’R) that gives off a pleasant smell. The following is an example of this reaction: The reaction above represents the formation of 3-methylbutyl ethanoate from ethanoic acid, 3-methylbutanol, and an acid catalyst.…

    • 1378 Words
    • 6 Pages
    Great Essays
  • Great Essays

    Quantification of Iron in Whole Grain Cereal Jacob Rickman and Yasmeen Coan Submitted to: Curt Zanelotti CHEM 1045, Experiment No. 12, April 15, 2016 LABORATORY WRITTEN REPORT Honor Code Signature: _________________ Objective In this experiment, we gained an understanding of the relationship between chemistry and food products while developing and enhancing good lab techniques. We applied dilution concepts to carry out the experiment.…

    • 1251 Words
    • 6 Pages
    Great Essays
  • Great Essays

    This means that the solution remains liquid even when the temperature is lower. Freezing point depression is when a solution has a lower freezing point than its solvent. This…

    • 1596 Words
    • 7 Pages
    Great Essays
  • Great Essays

    When calculating the quantitative solubility of the unknown compound in water, the amount of water that was measured in the hydrated cylinder and poured into the flask could have been greater than expected. This is more likely than less water being used because more solute was needed to saturate the solution than expected. Another error that could have occurred during this part of the experiment was that too much of the unknown compound was added accidently to the solution than could dissolve. Most of the error in this lab occurred during the quantitative analysis since all of the percent yields of the precipitate were over 100%. This miscalculation could have been caused by the beakers not being washed out thoroughly between each reaction or by the mass of KCl measured on the electronic scale being greater than exactly 0.5 grams.…

    • 1428 Words
    • 6 Pages
    Great Essays
  • Improved Essays

    Unknown #6 started its melting point at 132 ͒C and rapidly ended at 133͒C. The melting point range determined that the Unknown sample #6 is Urea. To determine the accuracy of the sample, I recorded the melting points of three substances : Unknown #6, 50-50 Mixture; includes .5 of the Unknown #6 and .5 of Urea, and Urea. Unknown #6 melted the same way as before, starting at 132͒ C and ending at 133͒ C. The 50-50 Mixture started its melting point at 132͒ C and ended at 133.2 ͒C. To establish that the Unknown sample #6 is Urea, I as well found the melting point range for Urea.…

    • 835 Words
    • 4 Pages
    Improved Essays
  • Superior Essays

    3.7 ANALYTICAL METHOD FOR ESTIMATION OF RALOXIFENE HYDROCHLORIDE IN HIGH PERFORMANCE LIQUID CHROMATOGRAPHY USING ACETONITRILE:0.05M AMMONIUM ACETATE (33:67) AS MOBILE PHASE 3.7.1 For Plain Drug Estimation Mode Reverse Phase HPLC Column C18 Detector UV Spectrophotometer Mobile Phase 0.05M Ammonium Acetate (pH 4): Acetonitrile Sample Raloxifene Hydrochloride in Methanol HPLC Flow Rate 1 mL/min Injection Volume 20µL Retention Time 4.6 min Λmax 289nm…

    • 777 Words
    • 4 Pages
    Superior Essays
  • Improved Essays

    Abstract This experiment involved an electrophilic aromatic substitution of bromobenzene. Two products were formed: 4-nitrobromobenzene (4-NBB) and 2-nitrobromobenzene (2-NBB). Utilizing column chromatography and recrystallization, separation and purification of the two products was obtained. The mass of 4-NBB, the para product, was 1.57 grams, while the mass of 2-NBB, the ortho product, was 0.80 grams.…

    • 1570 Words
    • 7 Pages
    Improved Essays
  • Superior Essays

    The Thermodynamics of Potassium Nitrate Dissolving in Water Introduction: This experiment focuses on thermodynamics or the study of heat and molecular randomness. It helps illustrate how and why potassium nitrate (KNO3) dissolves in water. When it dissolves, it dissociates into potassium (K+) and nitrate (NO3-) ions. These ions can also recombine into solid potassium nitrate. This reaction can reach a state where concentrations of ions remain constant or Ksp; which stands for the equilibrium concentration for the solubility product.…

    • 1221 Words
    • 5 Pages
    Superior Essays