Synthesis Of Cadmium Nitra-Hydrate Lab Report

Superior Essays
Destin Briggs
Lu Jack
Chem 4235
11/4/2017
Original Synthesis of Cadmium Nitrate Tetra-Hydrate
Cadmium nitrate tetra-Hydrate is an inorganic compound from the family of compounds with the general formula Cd (NO3)2.XH20, where X=4, hence the molecule has four molecules of water of crystallization in its structure. It exists as a salt but in its anhydrous state, it is known to be a volatile substance. It is a colorless substance as are all the compounds in the family of cadmium nitrates. Cadmium nitrate is a colorless, crystalline, inorganic compound that forms the toxic fumes produced when cadmium oxides are heated. It is an odorless white solid that is more dense than water.
Cadmium nitrate is prepared by first dissolving the metal cadmium or its oxide, carbonate, hydroxide in nitric acid them immediately
…show more content…
the mixture is then heated to a temperature of about fifty degrees Celsius, and 100g of fine powders of antimony sulfide are added in small amounts periodically to the heated mixture. After all of the crystals of antimony sulfide have been added to the mixture and evolution of hydrogen sulfide has subsided, the temperatures are adjusted to higher levels gradually until the resultant solution starts to boil (Karl‐Heinz and Magnus 20).
It is left to boil for an hour, adding boiling water periodically as it evaporates which keeps the flask contents at a constant level of about 500ml. after this, the solution is transferred to an evaporating basin and hot water added to a level where the solution appears as a very slight permanent turbid solution. The substance is then left boiling for five more minutes, filtered, then given time to flow into a larger vessel containing twenty liters of very cold water for cooling purposes (Karl‐Heinz and Magnus

Related Documents

  • Decent Essays

    Hazardous waste is dangerous to the environment and human health when not disposed properly, meaning cautions need to be taken seriously as chemistry students while working in lab. The objective of the Unknown White Compound experiment was to identify the compound by examining its chemical and physical properties. Identifying the unknown white compound to be potassium nitrate was achieved by completing the solubility test, flame test, pH paper test, ion test, pH probe test, conductivity probe test, and synthesizing silver nitrate and potassium chloride to form potassium nitrate. Uncertainty can be due to small contaminations from glassware not properly cleaned, molarity of chemicals not being exact, and not properly collecting the precipitate…

    • 159 Words
    • 1 Pages
    Decent Essays
  • Improved Essays

    Unknown Compounds

    • 695 Words
    • 3 Pages

    For this experiment, a group was employed by the Environmental Protection Agency as analytical chemists. Their goal was to identify an unknown compound that has been discovered in a landfill in their hometown. Once they identified the compound, they would then have to determine both the chemical and physical properties of the compound in order to inform the townspeople of any potential dangers. During the first week of lab, the group was given a small bottle containing an unknown white crystal-like substance.…

    • 695 Words
    • 3 Pages
    Improved Essays
  • Great Essays

    Then we did an anion test and discovered the compound reacted with chloride by producing a white precipitate. The precipitate that formed was an insoluble solid because Cl of NaCl reacted with Ag of AgNO3, creating a Cl- ion above the aqueous solution [3], results on Table 2. Finally we used a cation flame test, results on Table 4. When we burned the unknown substance the flame was a bright orange, yellow color. This was because the flame reacted with the Cl of NaCl causing…

    • 931 Words
    • 4 Pages
    Great Essays
  • Improved Essays

    represents a double displacement reaction. When zinc acetate, a clear liquid, and sodium phosphate, also a clear liquid, were combined in a test tube, they formed two different liquids. The reaction between the zinc acetate and the sodium phosphate happened almost immediately when combined together. One of the liquids was clear while the other was a milky white color. The clear liquid was sodium acetate and the white liquid is zinc phosphate, according to the MSDS.…

    • 95 Words
    • 1 Pages
    Improved Essays
  • Decent Essays

    Citrate Lab Report

    • 261 Words
    • 2 Pages

    Citrate: The citrate test gave a positive result, showing a dark blue color in the tube, caused by the alkaline conditions present, which is caused by the bacteria’s ability to utilize the citric acid present in the citrate slant. The positive result confirms the presecnce of the citrase enzyme. H2S Production: The H2S test yielded a positive result, giving rise to a black precipitate created by iron and H2S combining. Proving the presence of the desulfurase enzyme.…

    • 261 Words
    • 2 Pages
    Decent Essays
  • Improved Essays

    Cabr2: An Ionic Compound

    • 284 Words
    • 2 Pages

    CaBr2 is an ionic compound, because the second element is a non-metal so it will form an ionic compound. The next step in naming an ionic compound, is to name each component as if they were ions. The first component is a cation so you leave the name alone. The second component is an anion, so you change the ending of bromine to "-ide" and it’s becomes bromide. The last step is to combine the names so, CaBr2 becomes Calcium bromide.…

    • 284 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    Sodium Citrate Lab Report

    • 333 Words
    • 2 Pages

    The D-glucose serves to reduce the silver from Ag1- to Ag1+. The sodium citrate first reduces Ag1+ to Ag, and then functions to bind with the particle surface of silver nitrate particles to allow them to interact. Finally, silver nitrate can aggregate. The silver nitrate combined with D-glucose, sodium citrate, and heat forms an aggregate.…

    • 333 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    Sodium Citrate

    • 312 Words
    • 2 Pages

    The role of sodium citrate is to reduce silver nitrate to silver (1). The role of D-glucose was to reduce silver nitrate into just silver, while soluble starch stabilizes the nanoparticles by surrounding them to prevent aggregation (1, 2, 3). The 1 M NaOH, 1 M HCl, and 1 M NaCl caused Batch A to aggregate. The nanoparticles aggregated with these reagents because these are all strong bases or strong acids, which dissociates completely and interacts with the oxidized citrate that separate the nanoparticles, destroying the “citrate shield” away.…

    • 312 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    Density Lab Report Essay

    • 979 Words
    • 4 Pages

    Introduction Density measures the volume that a given amount of mass takes up. Usually, density has grams per unit volume as a unit. To find the density of an object, the object has to be measured and its mass has to be divided by its volume. Often times, density is used to identify substances, since different elements have specific densities. This experiment is made up of two sections; the first section measures the density of water and the density of an unknown substance.…

    • 979 Words
    • 4 Pages
    Improved Essays
  • Decent Essays

    Introduction The purpose of this experiment was to understand acid-catalyzed hydration of alkenes through the formation of exo-norborneol from the reaction of Norborene with acid and the excess of water. Acid-catalyzed hydration is useful in removing double and triple bonds; an unsaturated compound becomes reduced to a saturated compound in the presence of the acid catalyst, or water for this experiment. Hydration of alkenes is the result of acid-catalyzed addition of water to a carbon-carbon double bond. This leads to the formation of an alcohol.…

    • 505 Words
    • 3 Pages
    Decent Essays
  • Improved Essays

    Molecules Project 1: Chemiluminescence Luuk Adema & Ewout van der Veer S2794640 & S2680254 luukadema@hotmail.com & ewoutvanderveer@msn.com 31-10-14 F. Mecozzi, E. Hagting & M. van Zuylen Abstract Luminol was synthesized and the light intensity of its luminescence was tested. The yield of the synthesis was 55%. Measurements of the intensity of luminescence were done under standard and optimal conditions resulting in peak intensities of ±0.02 lux (standard) and ±0.03 lux (optimal). It has been shown that an increase in pH results in an increase in intensity with a maximum of pH=11.33.…

    • 1111 Words
    • 5 Pages
    Improved Essays
  • Improved Essays

    Iodometry Lab Report

    • 1421 Words
    • 6 Pages

    This will dissolve and oxidize copper into Cu2+. The solution was then heated to remove the brown NOx fume. This is necessary since NOx acts as an oxidizing agent and will oxidize I in the redox reaction to be observed. When all NOx fume is removed, H2SO4 was added and the solution was heated until white SO3 fumes appear. The addition of H2SO4 will drives off all nitrogen oxide gas that can interfere with the redox reactions. The SO3 vapor that is observed is an indication that all NOx has been driven off.…

    • 1421 Words
    • 6 Pages
    Improved Essays
  • Improved Essays

    Wittig Reaction Lab Report

    • 1084 Words
    • 4 Pages

    In this experiment, a Wittig reaction was performed in order to synthesize a mixtures of (E)- and (Z)-stilbene. Photoisomerization was then performed to isolate (E)-stilbene by transforming (Z)-stilbene into (E)-stilbene. The presence of the products throughout the experiment was monitored by 1H NMR. The final product was then characterized by 1H NMR, IR and its melting point. During synthesize of the product, the appearance of the reaction mixture changed.…

    • 1084 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Nitrates And Nitrite Essay

    • 1229 Words
    • 5 Pages

    Uses of Nitrates and Nitrites in food Nitrates and Nitrites in the food industry Nitrates and Nitrites or more commonly known as curing salt or pink salt, is usually used in foods such as hot dogs, sausages, ham, meat loaf, bacon and other deli meats. Nitrates and nitrites in the food industry are more commonly found in a charcuterie, which is a store that sells cooked meat in direct translation. We use nitrates and nitrites in our foods because they provide a more vibrant colour to red meat, it enhances flavour of the meat and helps to reduce bacterial growth therefore preserving the meat and extending its shelf life, allowing it to last longer, in addition, it helps to break down meats so that seasonings and flavour may be properly…

    • 1229 Words
    • 5 Pages
    Improved Essays
  • Superior Essays

    The Thermodynamics of Potassium Nitrate Dissolving in Water Introduction: This experiment focuses on thermodynamics or the study of heat and molecular randomness. It helps illustrate how and why potassium nitrate (KNO3) dissolves in water. When it dissolves, it dissociates into potassium (K+) and nitrate (NO3-) ions. These ions can also recombine into solid potassium nitrate. This reaction can reach a state where concentrations of ions remain constant or Ksp; which stands for the equilibrium concentration for the solubility product.…

    • 1221 Words
    • 5 Pages
    Superior Essays