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15 Cards in this Set

  • Front
  • Back

What is the goal of this lab experiment?

Isolate carvone from caraway seeds and spearmint leaves

Why is steam distillation important?

It is used to isolate oils and liquids with high boiling points

What are the 4 important requirements of steam distillation?

1. Non-reactive with water




2. Immiscible with water




3. Stable at 100 degrees celsius




4. Pressure is greater than or equal to 5 Torr at 100 degrees celsius

What is happening to the volatile components in the caraway seeds/spearmint leaves?

Co-distilling with the water vapor

Why will the distillate be cloudy?

Due to the carvone and water being immiscible

Are methylene chloride and water immiscible?

Yes

Is carvone soluble in methylene chloride?

Yes

What does immiscible mean?

Not soluble in all proportions

What is special about the total vapor pressure?

Always higher than the most volatile component

What is the most volatile component in steam distillation?

Water

What is special about the boiling point of the mixture?

Always lower than the lowest boiling point component (water at 100 degrees celsius)

What are the three techniques that can be used to analyze isolated oil?

1. Thin-layer chromatography




2. Baeyer Test




3. Smell

(R)-carvone and (S)-carvone are enantiomers. What does it mean to be enantiomers?

Non-superimposible mirror images

What is the one property that differs in enantiomers?

How they interact with plan polarized light (enantiomers rotate the plane of the light the same magnitude, but in opposite directions)

End

End