Titration

When trying to measure the 0.250 molar solution (of which is in water and sodium phosphate solution) in 500 mL, there are very specific steps in which you need to follow. Pouring the correct amount of the solution in the beakers is important, as to make sure that the solution is not over concentrated, or under concentrated. if you were to use a flask that had a different volume amount, and filled that flask up to (for example one flask with five hundred milliliters.) the full amount,the solution…

By measuring out two grams of our unknown, and heating it up until the difference of the mass of the test tube and the anhydrous residue subtracted to 0.002g, we were able to calculate the percent water in the two possible unknowns, and then our unknown, to figure out which unknown we were given. Since our percent water was 44.9%, we concluded that our unknown is Zinc Sulfate. A possible error as to why our calculated percent water was not exact to the theoretical percent water was most likely…

3.7.1. Effect of solvent and pH The influence of the solvent on Schiff base ligand L and its metal(II) complexes were studied. The results showed that the optimal solvent for Schiff base ligand L, Co(II), Ni(II) and Cu(II) complexes were CH3CN at λemi =320, 310, 316 and 330 nm, while the optimal solvent for Mn(II) complex was DMF λemi = 312 nm, as shown in Figure 7. The effect pH on the fluorescence intensity of Schiff base ligand L and its metal(II) complexes were investigated between…

Case study one 1. Principle of APTT: Platelet poor plasma (PPP) is incubated at 37 degrees Celsius then phospholipid (cephalin) and a contact activator (e.g.: Kaolin, ellagic acid) are added followed by calcium (all pre-warmed to 37 degrees Celsius). Addition of calcium initiates clotting and timing begins. The APTT measures the time required to regenerate thrombin and fibrin polymers via the intrinsic and common pathways. Reagents:  Platelet poor plasma (PPP)  Surface activator: example;…

Question 1: pH can be described as a measure of acidity or basicity (Alkalinity) of a solution. It is exactly equal in amount to the negative log of the concentration of hydronium(H3O+) ions. Due to the negative log relationship, increased hydronium ions transform to lower pH. When we add it to water, an acid releases hydrogen ion. Hydrogen ions in water unite with the water molecules to form hydronium ions, thereby lowering the pH and increasing the acidity of water. Water exposed to air is…

For the first synthesis reaction, camphene was converted to isobornyl acetate. In the fume hood, a sample of 1.36 g of camphene was added to a 25-mL round-bottomed flask along with a stir bar. To dissolve the camphene, 3.0 mL of glacial acetic acid was added into the flask. The flask was fastened onto a ring stand and immersed in a water bath that was on top of a stir plate. A thermometer wire was placed in the water bath to monitor the temperature throughout the experiment. After the camphene…

9. RESULTS Table 8: Pre Formulation Study S.NO API CHARACTERISATION RESULTS 1 Physical Appearance a white to slightly pink crystalline powder 2 Melting point 138-148 ºC 3 Bulk density 0.396 gm/ml 4 Tapped Density 0.421 gm/ml 5 Carr’s index/Compressibility index 5.94 6 Hausner’s Ratio 1.063 Conclusion: The value of compressibility index above 25%, 15-25%, less than10% indicates poor flowability, optimum flowability and high flowability respectively. As Efaverinz value is <10 so it exhibits…

Abstract For this experiment the amount of zinc in vitamin water had to be determined. To do this, three methods were applied. The first was by a calibration plot method, where zinc standards were prepared and from the absorbance of those standards a calibration curve was plotted, which in turn was used to determine the amount of zinc in vitamin water. The second method was standard addition. For this method, an un-spiked and spiked solution were prepared. The un-spiked solution only contained…

2. Materials and Methods: 2.1. Materials: Natural red, propidium iodide (PI), acridine orange and phosphate-buffered saline (PBS) were obtained from Sigma-Aldrich (St.Louis, MO). May–Grunwald–Giemsa stain was procured from Merck (Darmstadt, Germany). Fetal calf serum, Dulbecco's Modified Eagle Medium (DEMEM) and RPMI 1640 were bought from GIBCO/Life Technologies Inc. (Gaithersburg, MD). 2.2. Isolation and Proliferation of MSCs Bone marrow derived MSCs were isolated as described previously…

Radioactivity past paper assignment Question 1: In the fridge, from a previous experiment, there is a 50 mM [U-14C] glucose solution. A 20 uL aliquot was counted and gave 200 000 dpm. What is the specific activity of this preparation? 20 uL = 200 000 dpm (divide both sides by 20) 1 uL = 10 000 dpm Glucose = 50 mM = 50 mmol / uL = 50 umol/ uL = 50 nmol / uL Therefore in one uL = 50 nmol/ uL = 10 000 dpm (divide both side by…