Spectroscopy

3.4. Friction Characteristics of the NCD, MCD and boron doped NCD Coatings against Alumina Balls The friction coefficient curves of NCD, MCD and boron-doped diamond films sliding with Al2O3 balls are shown in figure 4, figure 5 and figure 6, respectively, for a sliding speed of 8 m/s and a load of 1N, 5N and 10N, respectively. Figure 4 (a), figure 5 (a) and figure 6 (a) show the friction coefficient of NCD, MCD and BDNCD at 1 N, respectively. Figure 4 (b), figure 5 (b) and figure 6 (b) show…

Q7) Describe how emission line spectroscopy is used in astronomy for the evaluation of star composition light years away from Earth. Please provide detailed information. The spectrum of stars consists of bright lines and dark lines. These lines are produced when the star emits or absorbs energy at specific wavelengths. Emission line spectroscopy is used in order to find out the star’s colour spectrum. The spectrum can be found by using a visible light telescope or by collecting radiation that…

When EPR spectroscopy is applied, two types of paramagnetic signals have been observed. The low field signal with g = 2.0023 and the other high field signal at g ˜1.96, both are associated with unpaired electrons trapped on oxygen vacancies. It is found that the intensity…

Experiment 5 Synthesis and NMR Spectroscopy of ethyl cinnamate Introduction: Wittig reactions involve the stereoselective synthesis of olefins from phosphonium ylides and aldehydes or ketones, where the carbonyl bond is converted to an alkene double bond.1 The variety of suitable reagents and the relatively mild experimental conditions facilitate their industrial applications, such as the synthesis of epoxides, esters, carotenoids and vitamin A.2,3 Specifically, the ester ethyl cinnamate is used…

resulting in a higher percentage. 2-NBB is less stable than 4-NBB, causing a lower percent yield. IR spectroscopy aids in determining the composition of a compound, allowing for identification. 2-Nitrobromobenzene was shown in product 1, but 4-Nitrobromobenzene could not be tested due to the small amount of product obtained. The two compounds can be distinguished by the peaks on the IR spectroscopy. 4-NBB contains an arene group, while 2-NBB contains an aldehyde/ketone group. The Thin layer…

Review of Stacking Interactions of Nucleobases: NMR Investigations by H. Sapper and W. Lohmann Introduction Nuclear magnetic resonance (NMR) spectroscopy is often a very useful tool to identify organic molecules based on the atomic nuclei interactions with their environment. Recent advances have made use of the technology in protein, nucleic acid, and complex natural products structure identification. [1, 2, 3] Its origins lie in the works of Felix Bloch and Edward Purcell, who used the…

Critical assessment of the article: Quantitative analysis by Auger Electron Spectroscopy 1 Introduction When the outer electron fills the vacancy left by an ionized electron in the inner shell, the released energy can be passed to another outer electron that causes further emitting of an electron with characteristic energy, this is the basic principle of the Auger electron spectroscopy (AES) [1]. Nowadays, AES is almost an indispensable tool in nanoscience research for its high surface…

History of Atomic Absorption Spectroscopy (AAS) Atomic Absorption Spectroscopy (AAS) was first proposed by Alan Walsh, later known as Sir Alan in 1955. Sir Alan worked in Melbourne for the Commonwealth Scientific and Industrial Research Organization (C.S.I.R.O.). This concept came to Alan Walsh in a flash of inspiration as he was gardening at his Melbourne home. This led to the invention that has since been labelled as one of the most significant achievements in chemical analysis for last…

5.2 Discussion 5.2.1 Comparison of the results from AFM and optical tweezers experiments 5.2.1.1 Different unfolding behaviors in AFM and optical tweezers experiments In chapter 3, we have studied AFV3-109 using single-molecule AFM. The results from optical tweezers are contradictory to the results from AFM. First, the unfolding force obtained by optical tweezers is much smaller than the force obtained by AFM. More importantly, in our previous study using AFM, the unfolding of AFV3-109 occurs in…

In this experiment, a series of reactions was performed in order to synthesize 6-ethoxycarbonyl-3,5-diphenyl-2-cyclohexenone, an a,b-unsaturated ketone. The two reactions performed in order to obtain this product were a Michael addition reaction and an Aldol condensation reaction. During this experiment, the reaction solution underwent several changes. Originally, the initial solution was light yellow and transparent. Once heated, the appearance of the reaction solution became bright yellow.…