Spectroscopy

Figure 1 shows the relationship between concentration and absorbance known as the Beer-Lambert law or calibration curve. The data from the made solutions in table 2 was used to create the graph. The graph has a linear trend line that predicts where a point would fall on the graph. The equation of the trend line is equation 7: y=0.9508x-0.0055 with a R2 value of 0.99943. This equation was used to find the true concentration of the made solutions as well as the unknown solution. The R2 value…

1 WRITTEN ESSAY Paragraph 1 The FePO4 crystal is examined at various temperatures ranging between 294K and 1073K by neutron powder diffraction. At relatively low temperatures, FePO4 adopts an α-quartz structure, which is tetrahedral. High pressures causes a phase change to a more dense octahedral structure, which is known as β-phase. The transition temperature is 980K. Cutoffs can be observed during the firstorder transition,. For α-phase, the increases in cell parameters…

Discussion/Scientific Explanation: In order to successfully analyze colas, one must become familiar with a Spectrophotometer 20. In order to do this, one must figure out determine the relationship between the wavelength of light absorbed and the color of a compound. Next, one must determine a way to relate the amount of light absorbed with the concentration of the solution. After gaining knowledge about these two parts of the lab, one will be able to determine how a Spectrophotometer 20 can be…

Introduction: The goal of this lab was for students to learn how to use a spectrophotometer to find the absorbance of four known copper (II) sulfate solutions, four copper (II) sulfate solutions that were created by dilution, and one unknown copper (II) sulfate solution. The purpose of this experiment was to help students learn how to use the Spec-20, which is a machine that measures the transmittance and absorbance of a solution, learn about the linear relationship between absorbance and…

WHAT IS NMR SPECTROCOPY? By definition, NMR spectroscopy is a research technique that makes use of the fact that certain atomic nuclei exhibit magnetic property to determine their chemical and physical properties for various uses that we’ll discuss later. History of NMR Spectroscopy Year Individual Discovery 1921 Stern and Gerlach Basis of quantum theory is confirmed by carrying out atomic and molecular beam experiments 1925 Ulhenbeck & Goudsmith Discovered the concept of spinning…

In our previous report, 21 we investigated the influence of formulation variables of clotrimazole-loaded cubic liquid crystalline nanoparticles. The composition of chitosan tailored cubic nanoparticles was optimized employing central composite design. The findings of Small angle X-ray scattering analysis confirmed the presence of D and P cubic phases in nanoparticles. Most importantly, considerable improvement in mucin binding was observed upon incorporation of chitosan owing to electrostatic…

Compare and contrast the crystal structures and crystal chemistry of quartz, α-FePO4 and β-FePO4. The structural evolution of FePO4 arises due to the deviation in temperatures from 294K to 1073K via a process known as the neutron powder diffraction. This happens when the temperature of 980K is reached to result in the α to β transition. There are however certain observations of discontinuities in structural parameters during this transition. The stark contrast is that during the α phase, there…

Observation & Calculations for Nanorefrigerant Graph of C.O.P. vs. Nanoparticle Concentration for Nanorefrigerant. C.O.P RESULTS WHEN NANOPARTICLE MIXED IN R134A & POE OIL Figure 5.1. Graph of nanorefrigerant C.O.P vs. nanolubricant C.O.P. 5.2. GRAPH OF PERCENTAGE CHANGE IN THE COP OF THE SYSTEM Figure5.2. Graph of percentage C.O.P of nanorefrigerantvs. nanolubricant. Here the result shows the percentage change in the C.O.P when the air conditioning test rig run on the nanorefrigerant and…

In the paper, FePO4 was studied in through neutron powder diffraction across a wide range of temperatures, and was found to have 2 states in general, the α (alpha) phase and β ( beta ) phase. The alpha phase exhibits a tetrahedral structure, which is similar to alpha quartz, and this occurs during generally low temperatures. In the case of this paper, the temperatures experimented on were between 294K and 1073K. The beta phase, however, is denser and exhibits a octahedral structure. The…

The FTIR spectrum of PVA/CS nanofiber was shown in Fig. 1(a). The band at 3255.32 cm−1 was corresponded to -OH stretching and the peaks at 1025.6 and 1450.04 cm−1 for the -C-O band. The peaks at 3445.32 cm-1, 2965 cm-1, 1640.01cm-1, 1598.7 cm-1, and 1361 cm-1 are due to amine NH symmetric vibration, C-H vibration, deformation vibration of the absorbed water molecules, stretching vibration of amino group of chitosan and vibration of C-H, respectively. The peaks at 890.1 and 1100 cm-1 was…