Sodium silicate

fitted with a heating mantle, mechanical stirrer, thermometer and reflux condenser, 0.5 mol of MOPE, 1.1 mol of epichlorohydrin and 300 mL of isopropanol were added to the flask. The mixture was heated to 60oC for 15 min. Subsequently 1.25 mol of sodium hydroxide in 500 mL water was…

The mixture in 2 was titrated against sodium thiosulfate placed in a 50.00 mL burette. 4. Steps 1-4 was repeated untill a difference of 0.01 mL is noticed in values taken. 2.0 LITERATURE REVIEW Experiment 1: Titration is a common laboratory method of quantitative chemical analysis that is used…

1.4 Effect of Microcrystalline Cellulose (MCC)Type Formula F12 was utilized to study the effect of changing the type of MCC(Avecil PH-101 ) as a carrier material instead of (Avecil PH-102) in F8 on the dissolution behavior of the prepared Zolmitriptan liquisolid ODTs. Although the DT of formula F12 (79 sec.) was greater than F8 (48 sec.) as in Table(18),the dissolution behavior of the formula F12 was faster than F8 as in Table (18) and Figure (48), this difference was non…

materials to be used in the formulation of soap and also to produce the average quality of soap bar using basic formulations from palm oil. Generally, soap is a salt of a compound and it is known as a fatty acid. Most soap is produced either by using sodium or potassium. Its molecule has a long hydrocarbon chain with a carboxylic acid group…

Experiment 1 and 2 Recrystallization: Purification of Solids and Melting points Purpose: In the fist experiment, impure Vanillin was purified through the process of recrystallization. Desired solutes were recovered through the technique of vacuum filtration, and then dried to take percent recovery In the second experiment, a percent recovery of the recrystallized Vanillin from the first experiment was performed. The percent recovery of Vanillin was 77.18% A mixed…

TRIS Hcl, NBT, NADH, Ethanol, PMS, l-ascorbic acid 1. The superoxide radicals is generated in 3 ml of TrisHCl buffer (16 mM, pH 8.0) containing 1 ml of NBT (50 μM), 1 ml NADH (78 μM) and ethanol extract of sample (25 – 50 μg). 2. The reaction was started by adding 1 ml of PMS solution (10 μM) to the mixture. 3. The reaction mixture was incubated at 25° C for 5 min, the absorbance was read at 560 nm using a spectrophotometer (Schimadzu UV-Vis 1700) against blank samples using l- ascorbic acid…

The unique composition and purity of as-deposited SnS2 thin films prepared with different precursor solution volumes from 5 ml to 25ml were determined by EDX analysis as shown in fig 5, which brought out the presence of Tin and Sulfur as elementary components. Two different peaks were observed in the spectrums from fig 5 relevant to the tin and sulfur. The EDX spectra show that the weight percentage for the film prepared at the precursor solution volume of 5 ml is 36.8% and 63.2%, which is…

relationship between the relative quantities of substances taking part in a reaction or forming a compound, typically a ratio of whole integers. In the lab that I did with my group we used stoichiometry to find out the decomposition of sodium biocarbonate. Sodium carbonate is just another name for baking soda, and that is what we used on our lab. Baking soda is also used in some food items, such as pancakes, waffles etc… When the baking soda is being heated the decompositon part occurrs and when…

Comparison of microbial growth between different groups Sodium Hypochloride Total Fishers exact test Endovac Laser Control p-value No Growth 5(50.0%) 8(80.0%) 0 15(37.5%) <0.001* <103 5(50.0%) 2(20.0%) 0 7(17.5%) 103 – 108 0 0 0 8(20.0%) >108 0 0 10(100.0%) 10(25.0%) Total 10 10 10 40(100.0%) *p<0.05 statistically significant p>0.05 non significant, NS Amongst the 10 samples evaluated for the endovac in conjunction with sodium hypochloride, 5 samples showed no growth…

Abstract: The purpose of this experiment was to prepare and standardize a sodium hydroxide solution as well as determine the molar concentration in as strong acid and the percent by mass of acetic acid in vinegar. We used volumetric analysis, also known as titration, in both experiments. The average molar concentration for NaOH was 0.2749 mol/L while the average molar concentration of the acid solution was .2493 mol/L.The average percent by mass of acetic acid in vinegar was found to be 12.3 %…