Phase 2 – Agarose Gel Electrophoresis 1. Obtain our four H, E, L, and P labeled micro tubes and place them on ice. 2. Set the micro pipet to 2.0 ul. 3. Transfer 2.0 ul blue dye to each of the four H, E, L, and P micro tubes. 4. Mix the four micro tubes by using this two-step method: * Place each tube briefly on the vortex to get the components to collect at the bottom of the micro tubes * Pulse spin the four micro tubes in the centrifuge to mix all of the components completely. 5.…
1.4 Effect of Microcrystalline Cellulose (MCC)Type Formula F12 was utilized to study the effect of changing the type of MCC(Avecil PH-101 ) as a carrier material instead of (Avecil PH-102) in F8 on the dissolution behavior of the prepared Zolmitriptan liquisolid ODTs. Although the DT of formula F12 (79 sec.) was greater than F8 (48 sec.) as in Table(18),the dissolution behavior of the formula F12 was faster than F8 as in Table (18) and Figure (48), this difference was non…
According to R.A Aitken, “An asymmetric synthesis may be defined as a synthesis in which an achiral unit is an ensemble of substrate molecules is converted to a chiral unit such that the possible stereoisomers are formed in unequal amounts.” It relates to any synthetic process that incorporates one or more new elements of chirality during a functional group transformation. Asymmetric synthesis involves the formation of chiral molecules. An object is said to be chiral, if it cannot be…
alloy and compounds of metals and nonmetal materials. Chemical vapor deposition can be defined as the deposition of a solid on a heated surface from a chemical reaction in the vapor phase [2]. Chemical vapor deposition belongs to the class of vapor-transfer processes. Differ from physical vapor deposition, CVD process includes chemical reactions. In the process, gaseous material change in to solid which means the process is…
Background : Stoichiometry is the relationship between the relative quantities of substances taking part in a reaction or forming a compound, typically a ratio of whole integers. In the lab that I did with my group we used stoichiometry to find out the decomposition of sodium biocarbonate. Sodium carbonate is just another name for baking soda, and that is what we used on our lab. Baking soda is also used in some food items, such as pancakes, waffles etc… When the baking soda is being heated…
The mixture was stirred, and a white precipitate of dicyclohexyl urea (DCU) was created after 15–30 min. The reaction was monitored by thin layer chromatography (TLC). After approximately 6–8 h, the precipitate was filtered and the filtrate was evaporated to dryness. The resulting residue was dissolved in acetone, filtered to additional remove any DCU, and evaporated…
CORROSION STUDIES WITH ANTIGONON LEPTOPUS IN 1M HCl S.Aejitha 1, P P.K.Kasthuri 2andGeethamani 3 1 Department of Chemistry, Asian College of Engineering & Technology, Coimbatore- 641110, India 2 Department of Chemistry, L.R.G.Government Arts College for Women, Tirupur- 638604, India 3 Department of Chemistry, Sriguru Engineering College of Technology, Tamil Nadu, Coimbatore -641110, India Correspondence should be addressed to S.Aejitha ,aejitha_subbaian@yahoo.co.in ABSTRACT The inhibition…
Diels-Alder Reaction Objective: The objective of this lab was to do a diels-alder reaction using anthracene, maleic anhydride, and xylene to create 9,10-dihydroanthracene, 10-, -succinic acid anhydride. Experimental: Anthracene (1.00g, 5.61x 10-3 mol), maleic anhydride (0.75g, 7.61x 10-3 mol), xylene (5mL, 4.71x 10-2 mol), and a stir rod were added into a round-bottomed flask. The round-bottom flask was then moved to the hood where the it was attached to a distillation column, placed on…
crystals for X-ray single crystal analysis was not obtained, to have reliable structural information, HR-TEM analysis of the product was carried out. The average size of the assembly calculated from HR-TEM measurement is found to be 2.8 nm which is in good agreement with the size of the previously reported Pd6L8 assembly where L is the non N-methylated (2.5nm, Fig. 2).9 As first step, to explore the catalytic activity of 1 in copper and phosphine free Sonogashira coupling reaction in water, we…
of equivalents of glycidol reacted with carbazole. Carbazole reacts with glycidol without catalyst. The process is exothermic and thus needs control of temperature. Reaction of carbazole with glycidol requires excess of glycidol, the best molar ratio is 1:7. When lower excess of glycidol is used, the carbazole precipitates from reaction mixture. This semiproduct obtained from carbazole and…