Fourier transform spectroscopy

Introduction: Limonene is a terpene that can be isolated from orange peels almost 100% in the (R)-(+)-limonene form. The essential oil from the orange peel belongs to terpenes, which are compounds that are made up of two or more five carbon units, named isoprene.1 The limonene is a monoterpene, which means it is made up of two isoprene units. Natural products are related compounds formally derived from isoprene units are terpenoids.3 The skeleton of terpenoids may differ from strict additivity…

Both IR and UV spectroscopy are methods of measuring the wavelengths absorbed by a tested material. IR spectroscopy measures the absorbance of the tested material in the infrared spectrum, the section of the electromagnetic spectrum with a lower frequency than that observed in the visible light spectrum. Conversely, UV spectroscopy measures the absorbance of the tested material in the ultraviolet spectrum, the section of the electromagnetic spectrum with a higher frequency than that observed in…

Joseph von Fraunhofer was a German optician and physicist who discovered and influenced how astronomers view the dark line spectrum, the spectrum of the sun and the diffraction of light. His discoveries turned him as a glassmaker with humble beginnings into a scientists whose discoveries would allow scientists after him to calculate the distances of stars and lead them to recognize that the universe is expanding. On March 6, 1787 in Straubing, Bavaria, Joseph Ritter von Fraunhofer was born into…

To begin the experiment, the Spec 20 was turned on to warm up for 15 minutes and set to maximum absorbance wavelength. Ten test tubes were then prepared. The Spec 20 was set to 0% and a test tube of blank solution (water) was wiped off and placed into the Spec 20. Transmittance was then set to 100% to calibrate the machine. Next, five test tubes were prepared and labeled with one of the standard solutions of 0.05 M, 0.1 M, 0.2 M, and 0.5 M CuSO4 in them. The Spec 20 was set to 600 nm and %…

Introduction: The goal of this lab was for students to learn how to use a spectrophotometer to find the absorbance of four known copper (II) sulfate solutions, four copper (II) sulfate solutions that were created by dilution, and one unknown copper (II) sulfate solution. The purpose of this experiment was to help students learn how to use the Spec-20, learn about the relationship between absorbance and concentration known as the Beer- Lambert law and see the relationship between moles, volume…

A spectroscope takes in light and breaks it into their own individual wavelengths, which are the colored lines we see. The light was produced by electrons, which each have their own quantum, or energy level. When we run a current through the atom, the electron gains energy and jumps to a higher level to its excited state. When they fall back to their ground state, they release their stored energy through the form of light. The line spectra for different atoms differ because they each have a…

technique of spectroscopy; spectroscopy can be defined as the science affiliated with the spectra produced when matter interacts with light. Lab 7 investigation 19, “What Factors Affect the Intensity of Color?” expands on the process of spectroscopy, and its relation to the molarity of a substance. The goal of this lab was to determine the effects of the intensity of color of a solution (2). Spectroscopy is frequently used in the medical field by using the process of infrared spectroscopy, which…

Review of Stacking Interactions of Nucleobases: NMR Investigations by H. Sapper and W. Lohmann Introduction Nuclear magnetic resonance (NMR) spectroscopy is often a very useful tool to identify organic molecules based on the atomic nuclei interactions with their environment. Recent advances have made use of the technology in protein, nucleic acid, and complex natural products structure identification. [1, 2, 3] Its origins lie in the works of Felix Bloch and Edward Purcell, who used the…

When EPR spectroscopy is applied, two types of paramagnetic signals have been observed. The low field signal with g = 2.0023 and the other high field signal at g ˜1.96, both are associated with unpaired electrons trapped on oxygen vacancies. It is found that the intensity…

greenhouse effect is what leads to global warming, but how does that happen? Let’s start with some historical analysis of the topic. The greenhouse effect (or at least a rough version) was originally thought of and recognized by Jean Baptiste Joseph Fourier in 1824. Starting with the concept that the earth’s atmosphere acts as an insulator for the sun’s energy and heat, Fourier’s idea was recognized and theorized into what is now the known as the greenhouse effect. A more thorough description…