of copper powder in other less concentrated amounts of nitric acid. This is as if the concentration of nitric acid is increased, then the amount of time taken for the copper powder to react will decrease, because nitric acid is a highly corrosive chemical and will therefore lead to a rapid and powerful reaction when it comes in contact with the copper powder, thus…
In pursuit of our continued interest in the development of solvent-free and green synthetic procedures, we decided to explore the use of tartaric acid catalyst for synthesis of polysubstituted quinolines via Friedlander condensation in high to excellent yields at 70 °C under solvent-free conditions. Initially the reaction between 2-aminobenzophenone (1.0 mmol) and dimedone (1.0 mmol), as the model reaction was examined in the presence varying amount of tartaric acid as catalyst and the results…
The synthesis of Aa-g-poly(MAA) involve the optimization of various reaction conditions like initiator concentration, monomer concentration, crosslinker concentration, solvent concentration and pH. After the optimization of various reaction parameters the replications were carried-out in triplicates for the reproducibility of the results and statistical of the results obtained. It was performed using the Statistical Package for Social Science (SPSS) version 10. Statistical results of the…
composite has been investigated. For that purpose, the PMMA samples with Al2O3 additive prepared with different percentages(0,15,25,35 and 45) wt.% and different thickness. The experimental results showed that the D.C electrical conductivity increased with increasing the alumina concentrations and temperature. Also the activation energy change with increasing of additional alumina. The dielectric constant, dielectric loss, A.C electrical conductivity are changed with change the concentration of…
4.2.4 Effect of Feed flow rate (Fgr) on Product Distribution An increase in the flow of gas oil means an increase in the velocity of the gas oil feed, also a decrease in the residence time of the gas oil in the riser; hence a rise in the conversion of gas oil and yields of the products is expected(Akpa et al. 2010). When the flow rate of gas oil is increased, there is an increase in the heat inflow into the reactor, rate of cracking reactions are high, feed also spends less time in the reactor…
derivative of the amino acid -carboxamide (VFCA-I toVII ) synthesized through coupling of N-Phthaloyl amino acid chloride derivative (2a-2g- synthesis reported in chapter-1) with 1-(2-amino-1-(4-methoxyphenyl) ethyl)cyclohexanol (VF-II). All the chemicals used are of laboratory grade and purchased from local commercial suppliers and used without further purification. Melting points determined…
Introduction and Overview: For this extended essay, I will be working on building and optimizing different sized water rockets to find out the optimum amount of fuel (water) for each the different rocket sizes. I will be measuring the ranges at which each rocket will fly to find out the optimum fuel level. A brief summary of water rockets: A water rocket is made up of a selection of parts to provide its successful launch: the nose cone which will make the rather snub-nosed end of the large…
1. Redox Catalyst Catalyst is defined as a substance that increases the rate of a chemical reaction without changing its chemical composition and affecting the standard Gibbs free energy, by lowering the activation energy of a chemical reaction. It does so by providing an alternative reaction pathway. In redox reaction, the key chemical event is the net movement of electrons from one reactant to the other. The oxidation state of atoms are changed. Transition metal is used as redox catalyst due…
Demitri Mendeleeve was a Russian chemist who invented the first periodic table in 1869. The periodic table he made was very different from the modern day periodic table we know today. Henry Moseley updated Mendeleev's version of the periodic table in 1915. This is more like the periodic table that we know and use today. The only difference is that there has been many more elements added. Mendeleeve also had predicted a lot of the characteristics and properties of elements that would fill up…
1. Chemical reactions involved in the oxidation of benzene (adapted from Lupușor et al., 1981) In order to achieve such an analysis, a simplified mathematical model of the reactor was used considering a pseudo-homogeneous, one-dimensional, plug-flow reactor. Model equations are presented in the Table 1 in terms of the mass balance of the considered chemical species, heat and moment balance, with the rate constants given in Table…