III. RESULTS AND DISCUSSIONS: A. Characteristics of Aluminum-Graphite composites and the in-situ reaction To examine the reaction condition of carbon flakes and Al powders, 4 wt. % carbon flakes were added to Al powders. Fig. 1 shows the DSC plot obtained during heating and cooling of the green compact from room temperature to 750 0C and from 750 0C to room temperature at a heating/cooling rate of 3 0C /min under argon gas atmosphere. From the DSC heating curve it is evident that the total…
Phase 2 – Agarose Gel Electrophoresis 1. Obtain our four H, E, L, and P labeled micro tubes and place them on ice. 2. Set the micro pipet to 2.0 ul. 3. Transfer 2.0 ul blue dye to each of the four H, E, L, and P micro tubes. 4. Mix the four micro tubes by using this two-step method: * Place each tube briefly on the vortex to get the components to collect at the bottom of the micro tubes * Pulse spin the four micro tubes in the centrifuge to mix all of the components completely. 5.…
When the drug within the liquisolid system is completely dissolved in the liquid vehicle, it is located in the powder substrate still in a solubilized state. Therefore they show improved release rate ,Thus, its release is accelerated due to its markedly increased…
According to R.A Aitken, “An asymmetric synthesis may be defined as a synthesis in which an achiral unit is an ensemble of substrate molecules is converted to a chiral unit such that the possible stereoisomers are formed in unequal amounts.” It relates to any synthetic process that incorporates one or more new elements of chirality during a functional group transformation. Asymmetric synthesis involves the formation of chiral molecules. An object is said to be chiral, if it cannot be…
alloy and compounds of metals and nonmetal materials. Chemical vapor deposition can be defined as the deposition of a solid on a heated surface from a chemical reaction in the vapor phase [2]. Chemical vapor deposition belongs to the class of vapor-transfer processes. Differ from physical vapor deposition, CVD process includes chemical reactions. In the process, gaseous material change in to solid which means the process is…
Background : Stoichiometry is the relationship between the relative quantities of substances taking part in a reaction or forming a compound, typically a ratio of whole integers. In the lab that I did with my group we used stoichiometry to find out the decomposition of sodium biocarbonate. Sodium carbonate is just another name for baking soda, and that is what we used on our lab. Baking soda is also used in some food items, such as pancakes, waffles etc… When the baking soda is being heated…
a reference standard correspondingly. Compatibility studies The compatibility of drug and polymers under experimental condition is significant precondition before formulation. Incompatibility between drugs and excipients can modify stability and bioavailability of drugs, thereby, moving its safety and efficacy. Study of drug–excipients compatibility is a vital process in the growth of a stable dosage form. Drug–excipients compatibility testing at an early stage helps in the assortment of…
CORROSION STUDIES WITH ANTIGONON LEPTOPUS IN 1M HCl S.Aejitha 1, P P.K.Kasthuri 2andGeethamani 3 1 Department of Chemistry, Asian College of Engineering & Technology, Coimbatore- 641110, India 2 Department of Chemistry, L.R.G.Government Arts College for Women, Tirupur- 638604, India 3 Department of Chemistry, Sriguru Engineering College of Technology, Tamil Nadu, Coimbatore -641110, India Correspondence should be addressed to S.Aejitha ,aejitha_subbaian@yahoo.co.in ABSTRACT The inhibition…
Diels-Alder Reaction Objective: The objective of this lab was to do a diels-alder reaction using anthracene, maleic anhydride, and xylene to create 9,10-dihydroanthracene, 10-, -succinic acid anhydride. Experimental: Anthracene (1.00g, 5.61x 10-3 mol), maleic anhydride (0.75g, 7.61x 10-3 mol), xylene (5mL, 4.71x 10-2 mol), and a stir rod were added into a round-bottomed flask. The round-bottom flask was then moved to the hood where the it was attached to a distillation column, placed on…
activity of 1 in copper and phosphine free Sonogashira coupling reaction in water, we optimised the conditions for the reaction between p-Iodonitrobenzene and phenyl acetylene in absence of copper(I) salt. It was observed that at a temperature of 50°C (among 25°C, 50°C and 80°C) the bases used, piperidine and Et3N (among NaHCO3, Na2CO3, K2CO3, KOH, Et3N and piperidine) give high yield under aerobic conditions (Table 1). Secondly, parallel reaction between phenyl acetylene and p-Iodonitrobenzene…