Acetic acid

The goal of this experiment was to use the technique of thin layer chromatography (TLC) to identify the active analgesic ingredient of Advil and monitor the transesterification of methyl salicylate from acetylsalicylic acid. The synthesized methyl salicylate was then purified using acid-base chemistry and analyzed using H NMR spectroscopy. Identification of a proper mobile phase to separate common analgesics used in over-the-counter pain relievers was essential in being able to determine the…

Introduction Acetone (dimethyl ketone, 2-propane, CH3COCH3), formulation weight 58,079, isthe simplest and the most important of the ketones. It is a colourless, mobile, flammableliquid with a mildly pungent and somewhat aromatic odour. It is miscible in all proportionswith water and with organic solvents such as ether, methanol, ethyl alcohol, and esters.Acetone is used as a solvent for cellulose acetate and nitrocellulose, as a carrier for acetyleneand as a raw material for the chemical…

Extraction of alkali from banana peels is known to depend on such parameters as ashing temperature, ashing time, soaking time and particle size of the ashed sample, soil type and variety. Alkali was extracted from three Nigerian grown banana peels namely: Saaro, Oloosun and Paranta for the purpose of determining the concentration of the extracted alkali. The concentration of the extracted alkali ranged from 0.02 to 0.10mol/dm3. The three varieties of the banana peels gave a maximum concentration…

3.3.9. Encapsulation efficiency of drug loaded NPs The encapsulation efficiency (EE) was determined by weighing the amount of unloaded drug recovered from lyophilization of the supernatant obtained after centrifugation of NPs. The drug encapsulation efficiency was calculated according to the following equation: Encapsulation efficiency (%) = (Winitial/Wfree)/Winitial *100%. Where, Winitial and Wfree are the weight of initial drug and the weight of free drug determined in the supernatant after…

Metin GUMUS et al.,[1]. In this study, hazelnut (Corylus avellana L.) kernel oil was tested and studied as an alternative fuel in diesel engines. The hazelnut kernel oil is made to undergo transesterfication process for reducing the viscosity of the oil. The processed hazelnut kernel oil possesses all the properties of biodiesel used in the diesel engine. The suitable transesterification reaction conditions for hazelnut kernel oil are volumetric ratio of the reactants in the ratio 1:5, reaction…

Complexation of Cyclodextrins Cyclodextrins (CDs) are most important carriers because of their semi-natural property as it is produced from a natural material i.e. starch, by simple enzymatic conversion. Solubility and dissolution rate of BCS class II drugs can be improved by addition or by complexation with hydrophilic carriers like cyclodextrins. Cyclodextrins have the capability to form inclusion complexes with the guest molecules i.e. poorly water soluble drugs. The formed inclusion complex…

Abstract: Distillation is the process of vaporizing a substance or a mixture; condensing it through the water condenser and then collecting it in the receiving flask1. In this experiment, fractional distillation is used to separate organic compounds that have a minuscule difference of their boiling points. The objective of this experiment is to purify and separate ethanol and water by fractional distillation to achieve the 95% of ethanol and 5% of water; then determine…

Witek-Krowiak et al., (2010) researched on the use of peanut shell to remove heavy metals from water solution. Cu (II) and Cr (III) ions were the heavy metals in this research, using Langmuir, Freundlich, Redlich–Peterson and Sips models to examine data gotten from the tests. The preparation of the bio sorbent material (peanut shell) was prepared by washing with pipe and refined water for about 1-2hrs to remove dirt and colour, the washed peanut shells were dried in an oven for a day then mashed…

3. Preparation of microemulsion:- Microemulsion was prepared by dispersing required quantity of Aripiprazole (15 mg/ml) in appropriate quantity of oil. The mixture was homogenized and to it, accurately weighed quantity of surfactant: cosurfactant blends was added in small portion with stirring. The blends were mixed thoroughly using magnetic stirrer and to it add dropwise double distilled water with continuous stirring around 10 min. compositions of ARP microemulsion shows in Table 1. 4.…

Abstract A spontaneous, one-pot strategy for the room temperature biosynthesis of gold nanoparticles (AuNPs) using Cocos Nucifera Linn (coconut palm) coir extract is described. The formation of AuNPs was observed within 30s of reaction time between the metal precursor and coir extract. The bioextract acted as both reducing agent and a stabilizer. The influence of various experimental parameters such as % volume fraction of coir extract, concentration of metal precursor, contact time and solution…