Abstract In this paper CuO-NH-NH2 nanoparticle was synthesized and used to remove anionic dyes from single and binary systems. The scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), Energy-dispersive X-ray spectroscopy (EDAX) and X-ray diffraction (XRD) were used to characterize the nanoparticle. Direct Red 80 (DR80) and Direct Green 6 (DG6) were used as anionic dyes. The effect of adsorbent dosage, dye concentration and pH on dye removal was evaluated. Kinetic…
of solvent-free and green synthetic procedures, we decided to explore the use of tartaric acid catalyst for synthesis of polysubstituted quinolines via Friedlander condensation in high to excellent yields at 70 °C under solvent-free conditions. Initially the reaction between 2-aminobenzophenone (1.0 mmol) and dimedone (1.0 mmol), as the model reaction was examined in the presence varying amount of tartaric acid as catalyst and the results are presented in Table 1. The best result was achieved by…
Pharmacology 1 Major Assignment Salbutamol The chemical name of salbutamol is 1-(4-hydroxy-3-hydroxymethylphenyl)-2-(t-butylamino)-ethanol sulphate, chemical structure is (C13H21NO3)2 • H2SO4 and molecular weight is 576.7g/mol Generic Name: albuterol Commonly used brand name(s): Available doses and dosage forms: Oral salbutamol: Adults and Children over 12 years: Usual starting dosage of salbutamol is 2mg or 4 mg 3 or 4 times a day. A dosage exceeding 4 milligrams of salbutamol 4 times…
Sterile Saline (0.9% w/v NaCl) Dissolve 9.0gm of NaCl in 1000ml water and dispense 9.0ml of the solution into 20ml test tubes. Autoclave the tubes as per the validated cycle and cool to room temperature. Sterile saline with polysorbate 80: Dissolve 9.0gm of NaCl in 1000ml water and add .5gm of tween 80 to the resulting saline solution, dispense 9.0 ml of the solution into a number of 20ml test tubes. Autoclave the tubes Preparation of Inoculums and its Standardization: 1) Take loop full of…
The role of oxysterols in human body and disease 1. Introduction Oxysterols are 27-carbon derivatives of cholesterol created by spontaneous or enzymatic oxidation (Figure 1, (Brown and Jessup, 2009)). The oxidation of cholesterol occurs either on the side chain or on the sterol core. Side chain oxidation generates, e.g., 24-hydroxycholesterol (24-HC), 25-hydroxycholesterol (25-HC) or 27-hydroxycholesterol (27-HC) while the core oxidation gives rise to ring oxysterols, mostly ring-B oxysterols,…
In this study, we use the modified organo nanoclay as a new sorbent for separation and preconcentration trace amounts of Au(III) in aqueous solutions. Nanoclay was modified with 5-(4'-dimethylamino benzyliden)-rhodanine. Modified nanoclay was used as a solid sorbent for separation and preconcentration trace amounts of Au(III) ions. The sorption of gold ions was quantitative in pH range of 2.0 to 6.0, whereas quantitative desorption occurs instantaneously with 6.0 mL of 1.0 mol L-1 Na2S2O3. The…
the remaining catalase into a new medicine cup and heat it in the microwave. Repeat the above procedure 3 times using the heated enzyme to dip circles into and record data. Finally take the rest of the original catalase and add a drop of hydrochloric acid to it. Repeat the above procedure 3 times using the acidified enzyme to dip the circles into and record data. b) Take a test tube and place a…
This lab used techniques in steam distillation to extract crude oil from cloves. The cloves were boiled in a round bottom flask and using a hydrodistillation apparatus, the crude oil was separated from the cloves and sent into a clean flask. This step was used to separate the essential oils from the cloves (Setzer, W., 2008). The distillate was poured into a separatory funnel and extracted three times with dichloromethane to extract the water. After being extracted three times, a fifth of the…
first step of the experiment, m-toluic acid reacted with thionyl chloride to form the acid chloride derivative of m-toluic acid. In this reaction, the carboxylic acid is first converted into an acyl chlorosulfite intermediate, replacing the –OH of the acid with a better leaving group. The acyl chlorosulfite then reacts with a nucleophilic chloride ion, at which point the chlorosulfite leaves in the form of sulfur dioxide and chloride ion. The remaining acid chloride then reacts with diethylamine…
separated by parts. First, a filter paper was used to separate the salt and water from the chalk and sand. is the filtration process, a separation technique using a filter paper to separate solid particles in a liquid. Second, acid dissolution, using HCl (Hydrochloric acid) that will react with calcium carbonate to produce CO2 , thus creating a chemical reaction. Afterwhich, evaporation was used to separate the table salt from the water. Specifically, this technique entails the changing of the…