Acetic acid

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    Introduction The ferric chloride test is used to determine the presence of phenols in a given sample or compound (for instance natural phenols in a plant extract). Enols, hydroxamic acids, oximes, and sulfinic acids give positive results as well. The ferric chloride test can be used to detect metabolites in urine in case of inborn error of metabolism such as phenylketonuria. In addition,the Ferric Chloride test can be used to detect salicylates in urine after an aspirin overdose.1 Background…

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    Lead concentrations can be measured in various body tissues or by measuring the biomarkers of the toxic effects of lead. The concentration of lead in the body has been measured in blood, bone, nails, hair, teeth, urine, faces and saliva for screening and diagnostic purposes. In all samples, specimen collection, storage and processing must be meticulously performed to avoid contamination of the samples with lead in the surrounding environment. Teeth, nail and bone reflect long term exposure to…

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    Mole Ratios Lab Report

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    experiment tested why mixing reactants in different mole ratios affected the amount of the product and the amount of each reactant that is left over. To solve the problem, the lab contained reacting sodium bicarbonate(baking soda) and acetic acid(vinegar) in different ratios and seeing if the product changed. The data suggests that the higher ratio of baking soda to vinegar creates the most product. For the ratio 3:1, the final grams of sodium acetate(product) was 0.09, the product…

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    Acetylsalicylic Acid from Salicylic Acid Shultz, Joshua T. Chemistry 2210L Data Figure 1. Esterification of Salicylic Acid to Yield Acetylsalicylic Acid Figure 2. Acetyl Group Table 1. Reference Data, Experimental Volumes, Yields, and Melting Points Melting Point of Salicylic Acid 158° C Melting Point of Acetylsalicylic Acid 138° C - 140° C Initial Mass of Salicylic Acid 0.510 g Theoretical Yield of Acetylsalicylic Acid 0.665 g Experimental Yield of Acetylsalicylic Acid 0.524 g…

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    In the foregoing paper, the author reported that ethyl ester of highly unsaturated fatty acid freshly obtained from cuttle fish oil showed quite the same good nutritive effect as oleic acid ester for rat, while the acid exposed to air was proved to be extremely toxic. Since it seems to be most plausible that the toxicity is concerned with the formation of peroxide by autoxidation of unsaturated fatty acid, the author determined the amount of peroxide. The result proved. this was just the case,…

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    Cation Flame Test

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    Using qualitative analysis, two cations in an unknown solution was identified. After repeated mixing, centrifugation, and decanting, lead was confirmed in Part A and barium in Part B. In Part C, different colored flames of metal species were observed using cation flame tests. Formula unit, total ionic, and net ionic equations were then composed for the identified cations. If the experiment were to be repeated, step 13 could be ommitted as barium was already confirmed in step 12 with the…

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    slowly. In order to speed up the process, hydrochloric acid (H+) was used as a catalyst. A catalyst is a substance that can speed up a reaction by lowering the activation energy of the reaction. It does this by changing the mechanism of the reaction and providing more energetically favorable elementary steps that would otherwise not exist without its presence. In addition, a catalyst does not get used up in the reaction. In this case, hydrochloric acid reappears in the products of the reaction…

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    place. The temperature dropped about 6 degrees Celsius. The remaining solution was a filmy and diluted. The result was sodium acetate dissolved in water. This reaction was a double displacement reaction. The sodium bicarbonate reacted with the acetic acid vinegar and produced sodium acetate, water, and carbon dioxide. The carbon dioxide escaped from the solution leaving water and sodium acetate.…

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    Camphene Synthesis

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    to a 25-mL round-bottomed flask along with a stir bar. To dissolve the camphene, 3.0 mL of glacial acetic acid was added into the flask. The flask was fastened onto a ring stand and immersed in a water bath that was on top of a stir plate. A thermometer wire was placed in the water bath to monitor the temperature throughout the experiment. After the camphene dissolved, 0.50 mL of 8 M sulfuric acid (H2SO4) was added. To prepare for heating, a cork was placed upside down to cap the mixture and…

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    Synthesis ofp-[1-(p-Hydroxyphenyl)-1-(p-Methoxyphenyl)Ethyl]Phenol (HMEP) 0.2 mol of phenol was mixed with the solution containing 100 mL of acetic acid in 200 mL of concentrated hydrochloric acid in 500 mL five necked round bottom flask fitted with anoil bath, thermometer, mechanical stirrer, reflux condenser. The contents of the flask was stirred for a period of 15 min, the solution was heated to 65oC, 0.1 mol ofp-methoxyacetophenone was introduced into a dropwise to the solution for about 6 h…

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