Solubility Test Lab Report

Improved Essays
The unknown compound we received consisted of white crystal-like particles and was a solid at room temperature. During the smell test, we did not receive any indication of a distinct smell, thus concluding that the compound is ionic.

The solubility tests indicated that the compound was soluble in water, NaOH, and HCl and non-soluble in acetone and toluene as shown in Table 1. The compound was soluble in water indicating that the compound is either polar or ionic, but not soluble in toluene or acetone eliminating it being polar or nonpolar, making our compound ionic. The compound was also soluble in both NaOH and HCl, which are contradicting because a compound cannot be an organic acid and base at the same time. Further into the experiment we investigated the fault of the solubility tests.

The quantitative solubility test was inconclusive for any extra information to help with the
…show more content…
Both the sulfate and chloride reactions formed a white precipitate when the compound was added to 6 M HNO_3 and AgNO_3 for the chloride test and 6 M HCl and BaCl_2 for the sulfate test. There were no indications of the other anions in our compound. A brown ring did not form for the presence of nitrate, there was no indication of fizzing for the presence of carbonate, and no fruity smell for the presence of acetate. With this we can further conclude that our compound is either NaCl or Na_2 SO_4. We know this from the fact that if chloride is present in a compound and it is added to AgNO_3 then there will be a precipitate formed, known as AgCl. This also goes for the sulfate anion. If sulfate is present in a compound and is added to BaCl_2 then a 〖BaSO〗_4 solid will precipitate out. As shown in Table 2, we had both reactions form a precipitate and thus concluding that our compound has either of these anions

Related Documents

  • Improved Essays

    Elizabeth Lee James Poland CHEM 104A 21 September 2014 Discussion and Conclusion of Experiment #4: States of Matter Sleuth Discussion The results of this experiment enabled the experimenter to determine the identity of an unknown salt (#3) using ion-exchange chromatography by analyzing the inorganic salts of the unknown salt, which can be examined by acid-base titration using ion-exchange resin. The stationary phase is made up of acid groups which will attach to the resin, which is then rinsed down the column with water. The mobile phase contains the inorganic salt dissolved in a solvent, which is then added to the column. As it goes down the column, an exchange of H+ ions and cations occur. The solution collected at the bottom of the column contains the acid form of the inorganic salt.…

    • 539 Words
    • 3 Pages
    Improved Essays
  • Improved Essays

    In this experiment, identifying the acids, bases, or neutrality of the unknown substance in a specific set are used to find the actual substances. The following sets of substances could have been assigned: Set 1 - Silver nitrate (AgNO3), Manganese(II) nitrate (Mn(NO3)2), Barium nitrate (Ba(NO3)2), Hydrochloric acid (HCl), Sodium Hydroxide (NaOH); Set 3 - Silver nitrate (AgNO3), Barium nitrate (Ba(NO3)2), Hydrochloric acid (HCl), Sulfuric acid (H2SO4), Sodium Hydroxide (NaOH); Set 4 - Silver nitrate (AgNO3), Lead (II) nitrate (Pb(NO3)2), Hydrochloric acid (HCl), Ammonia (NH3), Water (H2O). From the substances above Hydrochloric acid (HCl) is the stronger acid, and Sulfuric acid (H2SO4) and Lead (II) nitrate (Pb(NO3)2 are the weaker acids. If the substance is not an acid nor a base, the substance is neutral. In each set there were three neutral compounds, one acid, and one…

    • 495 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    Goals The goal of the lab was to investigate the properties and structure of an unidentified compound that was discovered in a local landfill. The group was called in to help determine the chemical and physical properties of the compound so we can let the people of the town know so it can be taken care of properly with or without further precautions to be taken. Another goal of this project was to devise the synthesis of the unknown compound. Experimental Design In order to determine the correct identity of our unknown compound, we first started with a couple preliminary tests, which include physical state and smell.…

    • 757 Words
    • 4 Pages
    Improved Essays
  • Great Essays

    Then we did an anion test and discovered the compound reacted with chloride by producing a white precipitate. The precipitate that formed was an insoluble solid because Cl of NaCl reacted with Ag of AgNO3, creating a Cl- ion above the aqueous solution [3], results on Table 2. Finally we used a cation flame test, results on Table 4. When we burned the unknown substance the flame was a bright orange, yellow color. This was because the flame reacted with the Cl of NaCl causing…

    • 931 Words
    • 4 Pages
    Great Essays
  • Decent Essays

    If Unknown 31B were to be an amine, it would likely be soluble in HCl but not soluble in water or NaOH. The acidity from the HCl allowed the amine group to be protonated allowing Unknown 31B to be soluble. Water and NaOH are not acidic and therefore could not protonate the amine group and therefore not being soluble with an amine. It can also be that Unknown 31B contained five or more carbons making it less soluble in water due to longer chains; the longer the chain, the less the functional group has polar influence, decreasing its water…

    • 100 Words
    • 1 Pages
    Decent Essays
  • Improved Essays

    Unknown Compounds

    • 816 Words
    • 4 Pages

    Given an unknown compound in container 3, solubility tests, cation tests, anion tests, and conductivity tests can be used to determine the various properties of the unknown to then make a positive identification of the unknown. These results will not only show chemical and physical properties but also what the unknown compound might react with to form other compounds. After performing the four anion tests, a positive identification was able to be made showing that the unknown compound contained a chloride ion since a white precipitate was formed from the reaction (Table 1). The sulfate, nitrate, and carbonate tests all yielded negative results when no precipitate was formed. The reaction of the chloride anion is as follows: Cl-…

    • 816 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Communication /6 Problem #2 Use the chart you just created to answer the following questions. a) Which substance would be the most corrosive? /1 Sample number 2 is the most basic and corrosive substance between the four samples.…

    • 1333 Words
    • 6 Pages
    Improved Essays
  • Improved Essays

    Cabr2: An Ionic Compound

    • 284 Words
    • 2 Pages

    CaBr2 is an ionic compound, because the second element is a non-metal so it will form an ionic compound. The next step in naming an ionic compound, is to name each component as if they were ions. The first component is a cation so you leave the name alone. The second component is an anion, so you change the ending of bromine to "-ide" and it’s becomes bromide. The last step is to combine the names so, CaBr2 becomes Calcium bromide.…

    • 284 Words
    • 2 Pages
    Improved Essays
  • Great Essays

    Ethyl Cinnamate Synthesis

    • 921 Words
    • 4 Pages

    Experiment 5 Synthesis and NMR Spectroscopy of ethyl cinnamate Introduction: Wittig reactions involve the stereoselective synthesis of olefins from phosphonium ylides and aldehydes or ketones, where the carbonyl bond is converted to an alkene double bond.1 The variety of suitable reagents and the relatively mild experimental conditions facilitate their industrial applications, such as the synthesis of epoxides, esters, carotenoids and vitamin A.2,3 Specifically, the ester ethyl cinnamate is used as a flavouring agent and in perfumes. The diastereomers of the alkene are distinguished through Proton Nuclear Magnetic Resonance (1H NMR) spectroscopy, where the coupling constants of alkenyl protons are different for (E) and (Z) isomers.4…

    • 921 Words
    • 4 Pages
    Great Essays
  • Improved Essays

    Laboratory Techniques and Measurements Tiffany Abbe Introduction: In this lab I will be adapting more about how to utilize distinctive estimation instruments and comprehend the diverse procedures included. Figuring out how to ascertain temperature and length. Will likewise make estimations utilizing the SI frameworks for fixation, thickness, and volume. While having the capacity to reate arrangements of building so as to change focuses and densities as tock arrangement.…

    • 1009 Words
    • 5 Pages
    Improved Essays
  • Great Essays

    By combining the unknown compound with an acid, a base, and two salts, its reactivity was determined. Reacting the unknown compound with sulfuric acid (H2SO4) produced no visible reaction (precipitate), although the pH of the resulting solution was very acidic. Combining the unknown compound with sodium hydroxide (NaOH), a strong base, also had no visible reaction. However, the resulting solution was a lot more basic. Reacting the unknown compound with sodium nitrate (NaNO3), a salt, did not have a visible reaction nor did the pH of the resulting solution change.…

    • 1428 Words
    • 6 Pages
    Great Essays
  • Decent Essays

    The two reactants chosen for the lab are Lead (II) Nitrate and Sodium Sulfate which produces a precipitate, Lead (II)…

    • 289 Words
    • 2 Pages
    Decent Essays
  • Improved Essays

    The product was decanted from the anhydrous sodium sulfate crystals into another round bottom flask. This round bottom flask was pre-weighed and then weighed after the addition of the product for the weight of crude cyclohexene. A few drops of the pure product went into a GC tube for analysis. A few drops were added to a test tube and 2 drops of bromine were added for the bromine…

    • 614 Words
    • 3 Pages
    Improved Essays
  • Improved Essays

    Lab Report Cation Essay

    • 875 Words
    • 4 Pages

    If this experiment were to be repeated, another cation could be added for identification or a flame test could have been done with the solutions in Part A and Part B in order to determine the cation identity. In Part A of this experiment, after carefully following each procedure, lead was concluded to be the cation present in the #2 unknown aqueous solution. This was concluded because of the formation of a yellow powdery precipitate inside the solution during the sixth step. This was as expected.…

    • 875 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Conclusion: The the precipitation reactions lab eight out of the fourteen occurring reactions were precipitates. A precipitate means that a solid substance was formed or a substance that is not aqueous was formed. The reactions that did not form a precipitate were DNR, which means that they did not react. At station one barium chloride and potassium nitrate did not react but barium chloride and silver nitrate reacted to form barium nitrate and silver chloride. The precipitate at station one was silver chloride.…

    • 939 Words
    • 4 Pages
    Improved Essays