Chloride Anion Tests

Superior Essays
Discussion of Results
During the first week the goal was to determine the unknown compound. In order to determine the unknown compound, many tests were performed testing the solubility, pH level, conductivity, cations present (flame test), and the anions present in the compound. The anion test had positive results for the sulfate test due to the formation of a white precipitate, indicating the presence of a sulfate ion. For the sulfate test the unknown solution, potassium sulfate, and combining it with hydrochloric acid and barium chloride. If a sulfate anion was present in the unknown solution, then the anion would combine with the barium and form the precipitate, BaSO4, and the chlorine ion would combine with the unknown’s cation. In this case a sulfate anion was present in the unknown so the sulfate combined with barium in the form of a precipitate, and the potassium combined with the chloride ion as an aqueous solution. The same fundamentals are used when testing for a chloride anion. If a chloride anion is present, except in the absence of sulfate, bromide, and iodide, when the unknown solution is combined with 6 M HNO3 and AgNO3 the chloride anion will combine with the Ag and form a precipitate in the
…show more content…
After the unknown compound was stirred in acetone for three minutes it turned a milky color, but never dissolved. Since the unknown compound dissolves in water that would indicate the unknown is either a polar or ionic compound, which is true for potassium sulfate, as indicated on page 591. For the pH test it was determined that the unknown compound turned the pH paper an orange color similar to a pH of 4, meaning the compound was slightly acidic. The conductivity test it was determined that the compound had a resistance of 70,000

Related Documents

  • Improved Essays

    Elizabeth Lee James Poland CHEM 104A 21 September 2014 Discussion and Conclusion of Experiment #4: States of Matter Sleuth Discussion The results of this experiment enabled the experimenter to determine the identity of an unknown salt (#3) using ion-exchange chromatography by analyzing the inorganic salts of the unknown salt, which can be examined by acid-base titration using ion-exchange resin. The stationary phase is made up of acid groups which will attach to the resin, which is then rinsed down the column with water. The mobile phase contains the inorganic salt dissolved in a solvent, which is then added to the column. As it goes down the column, an exchange of H+ ions and cations occur. The solution collected at the bottom of the column contains the acid form of the inorganic salt.…

    • 539 Words
    • 3 Pages
    Improved Essays
  • Improved Essays

    9-Fluorenone Lab Report

    • 1277 Words
    • 6 Pages

    Reduction involves increasing the number of carbon hydrogen bonds by adding hydrogen across a double or triple bond which results in an increase in electron density at the carbon atom. Organic functional groups containing double and triple bonds which undergo reduction are unsaturated. The reduction of the double bond by addition of hydrogen atoms results in the product being fully saturated. Metal hydride reducing agents that have different reactivities toward specific functional groups are commonly used in chemical reductions.…

    • 1277 Words
    • 6 Pages
    Improved Essays
  • Improved Essays

    6.03 Calorimetry Lab

    • 1044 Words
    • 5 Pages

    To test the solution for Pb2+ and Ag+ ions, add 8 drops of 6 M HCl solution to Test Tube 1 and stir the mixture. If a white precipitate forms, then Ag+ and/or Pb2+. Centrifuge the test tube and add one more drop of 6 M HCl. If more precipitate does form, continue adding HCl one drop at a time until the supernatant (the liquid) remains…

    • 1044 Words
    • 5 Pages
    Improved Essays
  • Improved Essays

    Nt1310 Unit 6 Lab

    • 1594 Words
    • 7 Pages

    My group had been given a specific task to investigate according to the lab manual1. We were employed by the Environmental Protection Agency as chemists. Our task is to identify an unknown compound that was found in a nearby landfill. In this laboratory, the unknown compound was given to us by our TA. The main goal of this experiment was to correctly identify the unknown compound.…

    • 1594 Words
    • 7 Pages
    Improved Essays
  • Improved Essays

    The pH test will confirm if the compound is an acid or base. After we performed the previous tests, we created five reactions that we knew would react with our predicted compound in a certain way. We came up with one reaction that would result in a white precipitate, and in the other four the compound will not react and only dissolve in the solution. We completed this test for both our known and our unknown and compared results.…

    • 757 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Unknown Compounds

    • 695 Words
    • 3 Pages

    Once the solubility tests were finished, this provided numerical evidence that aided in determining the identification of the compound. From these three weeks of investigation, the group…

    • 695 Words
    • 3 Pages
    Improved Essays
  • Superior Essays

    Essay On Nitrate Test

    • 1176 Words
    • 5 Pages

    The unknown was also unable to utilize malonate as the sole source of carbon. Once the malonate test was done, there was a yellow color, which indicated that it was…

    • 1176 Words
    • 5 Pages
    Superior Essays
  • Great Essays

    Discussion and Scientific Explanations The main goals of this experiment was to find the unknown compound, to discover the compounds chemical and physical properties and create two synthesis of the compound and compare the two compounds. We found out our compound was ionic because the compound dissolved in water, but not in toluene or acetone by using a solubility test, results on Table 1 of the group lab report. On page 59 of the Cooperative Chemistry Laboratory Manual is a chart on suggested liquids and the inference if the compound is soluble [1]. When then checked the pH of the solution by using pH strip. The solution had a pH>7.…

    • 931 Words
    • 4 Pages
    Great Essays
  • Improved Essays

    Magnesium Chloride Lab

    • 1562 Words
    • 7 Pages

    Magnesium Chloride as a Deicer Emily Lekah Fall 2015 CHEM 1066 October 15, 2015 University of Minnesota Abstract The purpose of this experiment was to evaluate magnesium chloride as a deicer. To be a good deicer, a salt must be able to lower the enthalpy when is mixed with water. This will cause an exothermic reaction and release heat.…

    • 1562 Words
    • 7 Pages
    Improved Essays
  • Improved Essays

    Hydrate Lab

    • 805 Words
    • 4 Pages

    The substance was stirred until dissolved. The liquid solution produced a blue color as soon as the cupric sulfate dissolved. Prior to this 1.127 grams of Zinc was gathered along with Hydrochloric acid. Both the Zinc and Hydrochloric acid were poured in gradually creating a reaction. A stirring rod was used to stir this while the reaction occurred.…

    • 805 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Unknown Compounds

    • 816 Words
    • 4 Pages

    Given an unknown compound in container 3, solubility tests, cation tests, anion tests, and conductivity tests can be used to determine the various properties of the unknown to then make a positive identification of the unknown. These results will not only show chemical and physical properties but also what the unknown compound might react with to form other compounds. After performing the four anion tests, a positive identification was able to be made showing that the unknown compound contained a chloride ion since a white precipitate was formed from the reaction (Table 1). The sulfate, nitrate, and carbonate tests all yielded negative results when no precipitate was formed. The reaction of the chloride anion is as follows: Cl-…

    • 816 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    K2CrO4 was added in Step 12 and this was what indicated whether or not the sample from Part B contained barium or not. The chloride ion in potassium chromate bound to the barium cation and formed a precipitate, if there were any calcium cations present, they would have stayed in the liquid solution. If the substance in Step 12 remained cloudy, it would have been a sign for a false positive. This refers to a result that may not be correct, and if it were the case, a precipitate of barium may have been formed, but that does not mean it has to. After that step, the precipitate was dissolved in 6M HCl and 6M H2SO4 was added resulting in a white precipitate forming.…

    • 885 Words
    • 4 Pages
    Improved Essays
  • Great Essays

    When calculating the quantitative solubility of the unknown compound in water, the amount of water that was measured in the hydrated cylinder and poured into the flask could have been greater than expected. This is more likely than less water being used because more solute was needed to saturate the solution than expected. Another error that could have occurred during this part of the experiment was that too much of the unknown compound was added accidently to the solution than could dissolve. Most of the error in this lab occurred during the quantitative analysis since all of the percent yields of the precipitate were over 100%. This miscalculation could have been caused by the beakers not being washed out thoroughly between each reaction or by the mass of KCl measured on the electronic scale being greater than exactly 0.5 grams.…

    • 1428 Words
    • 6 Pages
    Great Essays
  • Improved Essays

    To determine the concentration of the sulfate, the precipitation of Barium sulfate is done first by adding the sulfate solution with hydrochloric acid, then heating while stirring it. Next is the washing and filtration of the Barium Sulfate precipitate, using a vacuum pump and a crucible. Lastly, is the drying and weighing of the precipitate by heating the crucible in the oven and cooling it in a desiccator.…

    • 1080 Words
    • 5 Pages
    Improved Essays
  • Improved Essays

    For example at station one, barium chloride reacted with silver nitrate yielding to barium nitrate and silver chloride. Barium nitrate is aqueous because all nitrates are soluble. Silver chloride is the precipitate because all chlorides expect silver and a few others are soluble, since silver is an exception silver chloride is insoluble. To determine which reactant out of the chemical reactions the solubility rules provided the guideline necessary to figure out which reactant is the precipitate. The reactions in this equation were all of the same type of chemical reaction.…

    • 939 Words
    • 4 Pages
    Improved Essays