For example, when transferring the unknown samples from the weigh boats to the flasks, students could only use the smallest amounts of water possible. With small amounts of water used to transfer the reagent to an equipment, came the possibility of having a less than 100% transfer. And because a 100% reaction is dependent on a 100% transfer, a less than 100% reaction would be observed during this experiment as well. Other factors that can influence a less than 100% reaction included the following: forgetting to add specific reagents when required (i.e, forgetting to add the starch indicator to the product before the titration phase), using the wrong amounts of reagents (i.e. 0.0600g KIO3 instead of 0.6000g KIO3) and not adding the reagents in the specific order given (i.e. adding the starch indicator before adding the ammonium fluoride during the beaker reaction of the unknown samples; ammonium fluoride caused the release of the copper
For example, when transferring the unknown samples from the weigh boats to the flasks, students could only use the smallest amounts of water possible. With small amounts of water used to transfer the reagent to an equipment, came the possibility of having a less than 100% transfer. And because a 100% reaction is dependent on a 100% transfer, a less than 100% reaction would be observed during this experiment as well. Other factors that can influence a less than 100% reaction included the following: forgetting to add specific reagents when required (i.e, forgetting to add the starch indicator to the product before the titration phase), using the wrong amounts of reagents (i.e. 0.0600g KIO3 instead of 0.6000g KIO3) and not adding the reagents in the specific order given (i.e. adding the starch indicator before adding the ammonium fluoride during the beaker reaction of the unknown samples; ammonium fluoride caused the release of the copper