Synthesis ofp-[1-(p-Hydroxyphenyl)-1-(p-Methoxyphenyl)Ethyl]Phenol (HMEP) 0.2 mol of phenol was mixed with the solution containing 100 mL of acetic acid in 200 mL of concentrated hydrochloric acid in 500 mL five necked round bottom flask fitted with anoil bath, thermometer, mechanical stirrer, reflux condenser. The contents of the flask was stirred for a period of 15 min, the solution was heated to 65oC, 0.1 mol ofp-methoxyacetophenone was introduced into a dropwise to the solution for about 6 h…
Table 1: Experimental data for standardization of iodine solution. Calculation of standardization factor Standardization factor = (mass of vitamin C titrated) / (Volume of iodine solution used) = (125g) / (41.3ml) = 3.03 mg vitamin C/ml iodine solution Experiment B: Vitamin C titration using fresh fruit sample to determine the content The tabulated experimental data for this experiment is shown below (Table 2). In this experiment, the amount of vitamin C was calculated by multiplying…
Background : Stoichiometry is the relationship between the relative quantities of substances taking part in a reaction or forming a compound, typically a ratio of whole integers. In the lab that I did with my group we used stoichiometry to find out the decomposition of sodium biocarbonate. Sodium carbonate is just another name for baking soda, and that is what we used on our lab. Baking soda is also used in some food items, such as pancakes, waffles etc… When the baking soda is being heated…
ABSTRACT The reactivity of acid base cements forming hydroxyapatite (HA) such as, β-tricalcium phosphate (β-TCP) and dicalcium phosphate dehydrate (DCPD). Amorphous calcium phosphates, prepared by precipitation from supersaturated solutions, can also react to form apatitic cements since they are thermodynamic unstable with respect to HA and have a setting reaction more independent of particle size. Calcium phosphate cement containing an antibiotic can be used for filling bone defects and to…
compound that forms the toxic fumes produced when cadmium oxides are heated. It is an odorless white solid that is more dense than water. Cadmium nitrate is prepared by first dissolving the metal cadmium or its oxide, carbonate, hydroxide in nitric acid them immediately…
phosphine free Sonogashira coupling reaction in water, we optimised the conditions for the reaction between p-Iodonitrobenzene and phenyl acetylene in absence of copper(I) salt. It was observed that at a temperature of 50°C (among 25°C, 50°C and 80°C) the bases used, piperidine and Et3N (among NaHCO3, Na2CO3, K2CO3, KOH, Et3N and piperidine) give high yield under aerobic conditions (Table 1). Secondly, parallel reaction between phenyl acetylene and p-Iodonitrobenzene were…
Discussion: Based off the results from this lab the student was able to determine whether the model cell and cell environment each represent a hypertonic, hypotonic or isotonic solution. The first solution cell and environment the student had, was water and sodium chloride. In this instance water was the model cell (what was in the dialysis tubing) and Sodium chloride was the surround environment (plastic cup). The initial weight of the model cell was 13.2g, but after sitting in the sodium…
hetero-pairs in BLOCK (Plot A) follows similar pattern as Shannon Entropy Method (Plot C). Second, diversity profile for substitution by a given residue follows a characteristic pattern (plot B and D). Positional diversity changes when BLOCK undergoes amino acid substitutions. It is maximum when a position in BLOCK, has maximum and fixed occurrence of a residue (here V, first residue) followed by multiple copies of a second one (here I, second residue) with or without others. When other residues…
Jessica Grandier Bio 204 section 201 Case Study 1a What are the normal values for PH, Erythrocyte count, Leucocyte count, Platelet count. ( 1 point each) The normal values for PH are 7.35-7.45, the normal erythrocyte count for males is 4.7 - 6.1*10^6 /ul million and for women it is 4.2 -5.4*10^6/ ul million, Leucocyte count is 4,800-10,00 mmm^3 of blood and normal platelet count is 150,00-450,00 platelet for microliters. 1b What are the terms used for increase and decrease in PH…
Introduction The ferric chloride test is used to determine the presence of phenols in a given sample or compound (for instance natural phenols in a plant extract). Enols, hydroxamic acids, oximes, and sulfinic acids give positive results as well. The ferric chloride test can be used to detect metabolites in urine in case of inborn error of metabolism such as phenylketonuria. In addition,the Ferric Chloride test can be used to detect salicylates in urine after an aspirin overdose.1 Background…