Acetic anhydride

Introduction 1.1 Polyurethane polyurethanes were first developed by Otto Bayer and coworkers in 1937. Shortly thereafter, Schollenberger and coworkers used formula modification to prepare elastomeric polyurethane products from Bayer's products that were like nylon or other engineering plastics in physical characteristics. PUs are widely used in coatings, flexible and rigid foams, elastomers, and composites. Reasons for the use of polyurethane coatings include: high performance characteristics…

sodium hydroxide solution as well as determine the molar concentration in as strong acid and the percent by mass of acetic acid in vinegar. We used volumetric analysis, also known as titration, in both experiments. The average molar concentration for NaOH was 0.2749 mol/L while the average molar concentration of the acid solution was .2493 mol/L.The average percent by mass of acetic acid in vinegar was found to be 12.3 % Introduction: The Purpose of experiment 9 was to prepare and standardize a…

ABSTRACT Dex-Ibuprofen–polyethylene glycol (PEG) conjugates (PEG-dex-Ibu) were organized and their prospective as a prolonged release method was investigated. PEG-Dex-Ibuprofen conjugates were synthesized as of Ibuprofen and PEG with 4000 Da molecular weights by esterification in the incidence of DCC and DMAP. The PEG-dex-Ibu conjugates were characterized by FT-IR, 1H NMR, and DSC analysis. The solubility revise in aqueous system showed an improvement within the solubility of conjugates. The…

Diels-Alder Reaction Objective: The objective of this lab was to do a diels-alder reaction using anthracene, maleic anhydride, and xylene to create 9,10-dihydroanthracene, 10-, -succinic acid anhydride. Experimental: Anthracene (1.00g, 5.61x 10-3 mol), maleic anhydride (0.75g, 7.61x 10-3 mol), xylene (5mL, 4.71x 10-2 mol), and a stir rod were added into a round-bottomed flask. The round-bottom flask was then moved to the hood where the it was attached to a distillation column, placed on…

Since suitable crystals for X-ray single crystal analysis was not obtained, to have reliable structural information, HR-TEM analysis of the product was carried out. The average size of the assembly calculated from HR-TEM measurement is found to be 2.8 nm which is in good agreement with the size of the previously reported Pd6L8 assembly where L is the non N-methylated (2.5nm, Fig. 2).9 As first step, to explore the catalytic activity of 1 in copper and phosphine free Sonogashira coupling reaction…

New method of synthesis of oligoetherols with carbazole ring Renata Lubczak Abstract: The new method of synthesis of multifuntional oligoetherols with carbazole ring suitable for obtaining the polyurethane foams of enhanced thermal resistance was presented. At the first step of the synthesis the carbazole was reacted with excess glycidol to obtain the product of (n +1) functionality, where n is number of equivalents of glycidol reacted with carbazole. Carbazole reacts with glycidol without…

The Difference between Detergent and Soap The reason for this case study is to dissect the Difference between detergent and soap. In this case study, I will define the meaning of the cleaning agents, I will give you an introductory, I will discover how they are made, I will discover how they work, and why one cleaning agents is better than the other. This case study will be designed using the descriptive scientific method. The meanings of Detergent and Soap A detergent is a substance that cleans…

Jessica Grandier Bio 204 section 201 Case Study 1a What are the normal values for PH, Erythrocyte count, Leucocyte count, Platelet count. ( 1 point each) The normal values for PH are 7.35-7.45, the normal erythrocyte count for males is 4.7 - 6.1*10^6 /ul million and for women it is 4.2 -5.4*10^6/ ul million, Leucocyte count is 4,800-10,00 mmm^3 of blood and normal platelet count is 150,00-450,00 platelet for microliters. 1b What are the terms used for increase and decrease in PH…

Effect of Organic Solvents on Particle Size When anti solvent was 0.4% (w/v) F68 aqueous solution, the effect of various good solvent was investigated. These organic solvents include ethanol, methanol, PEG 400, propylene glycol. The result as mention in Table 16 & Figure 27 showed that the particles prepared by methanol were the smallest (317 nm) among other organic solvents. Ethanol, PEG 400, and propylene glycol produced the particles having the mean particle size of 525nm, 1274nm, 864nm,…

The purpose and objective of this experiment was to determine the percent by mass of acetic acid within a sample of vinegar using volumetric analysis with the titration technique. The theory is that if the volume and molar concentration of the standardized sodium hydroxide (NaOH) solution is known, then the percent by mass of the acetic acid (CH3COOH) in vinegar can be calculated after a titration.1 Within this experiment, a NaOH solution was standardized with a primary standard acid of…