Then 0.12g of benzoyl peroxide was added. The flask was swirled until it was a homogenous mixture. Next, the reflux apparatus was set up.
After set up was completed, the round bottom flask was heated in a heating mantle attached to a transformer that was set to 80%. The reaction was heated until the reflux began. The reflux was maintained for 30 mins without the condensation ring going above 1/3 of the