Limiting Reagent

Improved Essays
The purpose of these calculations is to identify the limiting reagent and calculate the percent yield of the esterification reaction used to produce aspirin. This reaction was catalyzed by concentrated H2SO4, but since it is not consumed during the reaction, it does not affect the stoichiometric calculations. In order to determine the limiting reagent, the moles of reactants were calculated (Part A). Part B of the calculations illustrates the amount of aspirin produced by each reactant based on 1:1 mole ratio defined by the balanced equation of the reaction. According to these calculations, salicylic acid is the limiting reagent because it produces the least amount of aspirin. Thus, the limiting reagent, if fully consumed, dictates the theoretical

Related Documents

  • Improved Essays

    Aspro Clear Experiment

    • 251 Words
    • 2 Pages

    It is essential for pharmacists to be able to predict the theoretical rate kinetics of pharmaceutical products in order to determine its shelf life. As the shelf life is defined by (t90), which is the availability of greater or equal to 90% of the drug, it is important to discover the rate of degradation of a drug to ensure that the patients receive an adequate dose of the drug. In this experiment, the stability of the active ingredient of Aspro Clear is investigated to identify the rate of degradation at different temperatures, to determine the optimum temperature for the storage of medications like Aspirin. First order reaction is classified as a reaction that is dependent or directly proportional to the concentration of a single reactant.…

    • 251 Words
    • 2 Pages
    Improved Essays
  • Decent Essays

    Spacer Lab Report

    • 393 Words
    • 2 Pages

    General procedure: One equivalent of spacer was coupled using 2.4 equivalents of inhibitor, 0.18 equivalents of copper sulfate, 0.36 equivalents of (+)-sodium-L-ascorbate, in a mixture of 10% H2O in DMF, 24 mL/mmol spacer. The mixture was placed in the microwave for 30 minutes at 80oC Pro6 Spacer (10) (30 mg, 0.036 mmol) and 18 (36 mg, 0.087 mmol) were dissolved in 778 µL DMF. Copper sulfate (1.62 mg, 0.006 mmol) and sodium-L- ascorbate (2.57 mg, 0.013 mmol) were dissolved in 86 µL H2O. The two solutions were combined in a microwave tube and put in the microwave for 30 minutes at 80oC. The solvent was evaporated under reduced pressure.…

    • 393 Words
    • 2 Pages
    Decent Essays
  • Improved Essays

    Experiment 11: Peptides and Amino Acids The purpose of this experiment was to study the amino acid composition of artificial sweeteners and then observe simple acid and base catalyzed reactions of the amino acid and artificial sweetener aspartame. This was achieved by performing a TLC analysis using ninhydrin as an indicator to observe the composition of the amino acid as well as two of the components that make up aspartame. This is followed by the addition of an acid or base to aliquots of diet sodas to examine the resulting reactions and compare them to a known hydrolyzed aspartame sample. The most common method of synthesizing amides is through the reaction of a primary or secondary amine with a carboxylic acid derivative.…

    • 882 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Esterification Lab

    • 596 Words
    • 3 Pages

    In the Fischer approach, an acid is used in order to allow the esterification to occur. Gas chromatography separates compounds by their elution time. Data and Results The compound in the gas chromatograph exhibited a retention time of 3.68 minutes.…

    • 596 Words
    • 3 Pages
    Improved Essays
  • Improved Essays

    Experiment 7 Electrophilic Aromatic Substitution Of Salicyamide Name: Lidia Santiana Palha Student number: s3333523 Email-address: lidiapalha@gmail.com Name of demonstrator: H.Helbert Reaction Equation Summary Salicylamide and sodium iodide are dissolved in ethanol, and stirred and cooled to 0. After that household bleach was added while stirring vigorously, solution changed from colorless to pale yellow. Sodium thiosulphate and hydrochloric acid were added aswell.…

    • 960 Words
    • 4 Pages
    Improved Essays
  • Improved Essays

    Aspirin And Acetaminophen

    • 356 Words
    • 2 Pages

    In order to extract aspirin, caffeine, and acetaminophen from a tablet of pain medication acid and base extraction techniques were used to exploit the differences in solubility between the components. This is achieved by using a separatory funnel and three different solvents, 4M HCl which separated the caffeine, deionized water which separated the acetaminophen, and 5% wt/vol NaHCO3 which separated the aspirin. Once the solution of the crushed tablet and ethyl acetate was mixed with a solvent in the funnel two immiscible layers will form. In the case of the aspirin separation, the carboxylic component will be attracted to the basic NaHCO3 layer, effectively separating it from the other components. This is the same with the other components and their corresponding solvents.…

    • 356 Words
    • 2 Pages
    Improved Essays
  • Decent Essays

    5-Iodosalicylamide

    • 284 Words
    • 2 Pages

    The purpose of this lab was to iodonize salicylamide and characterize the product in order to determine its structure. The crude product of this reaction was recrystallized using ethanol. The white crystalline product was isolated using vacuum filtration and characterized. The percent yield of this reaction was determined to be 39%. The observed experimental melting point of the product was determined to be 235-137 oC. When compared to the literature melting point 228 oC of the predicted product, 5-iodosalicylamide, it can be concluded that the product is very pure.…

    • 284 Words
    • 2 Pages
    Decent Essays
  • Improved Essays

    Asa Synthesis Lab Report

    • 300 Words
    • 2 Pages

    The purpose of the experiment was about recrystallization of crude ASA from crude ASA, then analyze the yield and melting point of Recrystallized product, test for Purity of Recrystallized ASA by using thin layer chromatography and analysis of Recrystallized Acetylsalicylic Acid by Spectroscopy to compare these results with another experiment about creating an Aspirin from Salicylic Acid. In this experiment, 0.1241 gram of Recrystallized ASA was produced from 1.1754 gram of Crude ASA and the yield of reaction is 10.56%. This yield is lower than the yield by creating an Aspirin from Salicylic Acid because the crystallized product is purer because we did not add another chemical in. For the melting point of recrystallized ASA, Mel-temp was used…

    • 300 Words
    • 2 Pages
    Improved Essays
  • Improved Essays

    The percent yield was less than one hundred percent because the reaction did not go to completion, and some of the product may have been lost during transition steps. For future experiments, it would be interesting to synthesize the compound that is made by Ibuprofen. This is a drug that has similar medical uses as a fever and pain reducer. Additionally, it would be interesting to compare the synthesized acetaminophen and the synthesized Ibuprofen under the IR spectrum and determine the different functional groups associated with the two…

    • 617 Words
    • 3 Pages
    Improved Essays
  • Decent Essays

    Grignard Limiting Reagent

    • 203 Words
    • 1 Pages

    The limiting reagent was found to be benzophenone and the theoretical yield was found to be 0.00598 mols of triphenylmethanol. The percent yield of the crude and pure product of triphenylmethanol was calculated to be 32.05% and 27.4% respectively.…

    • 203 Words
    • 1 Pages
    Decent Essays
  • Decent Essays

    Peroxidase Lab

    • 172 Words
    • 1 Pages

    This laboratory consisted of knowing the different effects of adding an enzyme and adding a substrate to a chemical reaction. Also by increasing or decreasing the temperature of a reaction as well as adding an inhibitor to test the enzymatic activity that would take place in the reaction. With the prior knowledge we conclude a hypothesis for this experiment. Which is the concentration for substrate will increase as well as the rate of reaction. As the temperature increases the rate of reaction increases too.…

    • 172 Words
    • 1 Pages
    Decent Essays
  • Decent Essays

    Purpose The question being explored in this experiment is how temperature affects the rate of reaction of Alka-Seltzer, or effervescent tablets. The purpose of this is to see whether hotter temperatures or cooler temperatures cause the reaction to be quicker. Effervescent tablets are used to orally distribute medicine for patients and consumers (Laboratories SMB). By adding the tablets to water, the medicine is released into the solution, allowing the consumer to easily drink the solution and take the drugs needed for their health (Haack & Köberle).…

    • 233 Words
    • 1 Pages
    Decent Essays
  • Decent Essays

    Experiments involving chemical reactions can be performed using simple household ingredients and products such as baking soda and vinegar. When baking soda (sodium hydrogen carbonate) reacts with ethanoic acid which is found in vinegar in a 1:1 ration, the reaction will produce three different products which are water, carbon dioxide and Sodium acetate. The reaction is: NaHCO3 + HC2H3O2 → NaC2H3O2 + H2O + CO2 In the experiment, the quantitative relationship between the two reagents which is the limiting reagent and which is the excess reagent will been found.…

    • 503 Words
    • 3 Pages
    Decent Essays
  • Decent Essays

    Introduction The purpose of this experiment was to understand acid-catalyzed hydration of alkenes through the formation of exo-norborneol from the reaction of Norborene with acid and the excess of water. Acid-catalyzed hydration is useful in removing double and triple bonds; an unsaturated compound becomes reduced to a saturated compound in the presence of the acid catalyst, or water for this experiment. Hydration of alkenes is the result of acid-catalyzed addition of water to a carbon-carbon double bond. This leads to the formation of an alcohol.…

    • 505 Words
    • 3 Pages
    Decent Essays
  • Improved Essays

    Abstract: The objective of this experiment was to synthesize aspirin from salicylic acid and acetic anhydride. The general theory behind this experiment was to study the synthesis of a drug from organic materials. During the experiment, esterification had occurred between reactants salicylic acid and acetic anhydride. Then, phosphoric acid would catalyze the reaction and water would be added to decompose the remaining acetic anhydride. Through the process of filtration, aspirin crystals were collected and separate from the liquid acetic acid-water solution.…

    • 993 Words
    • 4 Pages
    Improved Essays